Published October 23, 2015 | Version v1
Journal article Open

Evaluation of Thermal and Physical Properties of Magnesium Nitride Powder: Impact of Biofield Energy Treatment

  • 1. Trivedi Global Inc.

Description

Magnesium nitride (Mg3N2) has gained extensive attention due to its catalytic and optoelectronic properties. The present investigation was aimed to evaluate the effect of biofield energy treatment on physical and thermal properties of Mg3N2 powder. The Mg3N2 powder was divided into two parts i.e. control and treated. The control part was remained as untreated and the treated part was subjected to the Mr. Trivedi's biofield energy treatment. Subsequently, the control and treated Mg3N2 samples were characterized using differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and X-ray diffraction (XRD). The DSC results showed the specific heat capacity of 2.24 Jg-1°C-1 in control, which increased upto 5.55 Jg-1°C-1 in treated Mg3N2 sample. The TGA data revealed that the onset temperature for the formation of magnesium oxide, possibly due to oxidation of Mg3N2 in the presence of air and moisture, was reduced from 421.0°C (control) to 391.33°C in treated sample. Besides, the XRD data revealed that the lattice parameter and unit cell volume of treated Mg3N2 samples were increased by 0.20 and 0.61% respectively, as compared to the control. The shifting of all peaks toward lower Bragg angle was observed in treated sample as compared to the control. The XRD diffractogram also showed that the relative intensities of all peaks were altered in treated sample as compared to control. In addition, the density of treated Mg3N2 was reduced by 0.60% as compared to control. Furthermore, the crystallite size was significantly increased from 108.05 nm (control) to 144.04 nm in treated sample as compared to the control. Altogether data suggest that biofield energy treatment has substantially altered the physical and thermal properties of Mg3N2 powder. Thus, the biofield treatment could be applied to modulate the catalytic and optoelectronic properties of Mg3N2 for chemical and semiconductor industries. This record was migrated from the OpenDepot repository service in June, 2017 before shutting down.

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References

  • 1. Xue CS, Ai YJ, Sun LL (2007) Synthesis and photoluminescence properties of Mg3N2 powders. Rare Met Mater Eng 36: 2020-2022. 2. Veitch GE, Bridgwood KL, Rands-Trevor K, Ley SV (2008) Magnesium nitride as a convenient source of ammonia: preparation of pyrroles. Synlett 2008: 2597-2600. 3. Kojima Y, Kawai Y, Ohba N (2006) Hydrogen storage of metal nitrides by a mechanochemical reaction. J Power Sources 159: 81-87. 4. Nakano S, Ikawa H, Fukunaga O (1993) High pressure reactions and formation mechanism of cubic BN in the system BN Mg3N2. Diamond Relat Mater 2: 11681174. 5. Armenta MGM, Reyes-Serrato A, Borja MA (2000) Ab initio determination of the electronic structure of beryllium-, aluminum-, and magnesium-nitrides: A comparative study. Phys Rev B 62: 4890. 6. Murata T, Itatani K, Howell FS, Kishioka A, Kinoshita M (1993) Preparation of magnesium nitride powder by low-pressure chemical vapor deposition. J Am Ceram Soc 76: 2909-2911. 7. Toyoura K, Goto T, Hachiya K, Hagiwara R (2005) Structural and optical properties of magnesium nitride formed by a novel electrochemical process. Electrochim Acta 51: 56-60. 8. Movaffaghi Z, Farsi M (2009) Biofield therapies: Biophysical basis and biological regulations. Complement Ther Clin Pract 15: 35-37. 9. Priyadarsini K, Thangam P, Gunasekaran S (2014) Kirlian images in medical diagnosis: A survey. IJCA Proceedings on International Conference on Simulations in Computing Nexus 3: 5-7. 10. Aldridge D (1991) Spirituality, healing and medicine. Br J Gen Pract 41: 425427. 11. Hok J, Tishelman C, Ploner A, Forss A, Falkenberg T (2008) Mapping patterns of complementary and alternative medicine use in cancer: an explorative crosssectional study of individuals with reported positive "exceptional" experiences. BMC Complement Altern Med 8: 48. 12. Trivedi MK, Tallapragada RM (2008) A transcendental to changing metal powder characteristics. Met Powder Rep 63: 22-28, 31. 13. Dhabade VV, Tallapragada RM, Trivedi MK (2009) Effect of external energy on atomic, crystalline and powder characteristics of antimony and bismuth powders. Bull Mater Sci 32: 471-479. 14. Trivedi MK, Tallapragada RM, Branton A, Trivedi D, Nayak G, et al. (2015) Potential impact of biofield treatment on atomic and physical characteristics of magnesium. Vitam Miner 3: 129. 15. Trivedi MK, Nayak G, Patil S, Tallapragada RM, Latiyal O (2015) Studies of the atomic and crystalline characteristics of ceramic oxide nano powders after bio field treatment. Ind Eng Manage 4: 161. 16. Trivedi MK, Nayak G, Patil S, Tallapragada RM, Latiyal O, et al. (2015) Impact of biofield treatment on atomic and structural characteristics of barium titanate powder. Ind Eng Manage 4: 166. 17. Trivedi MK, Nayak G, Tallapragada RM, Patil S, Latiyal O, et al. (2015) Effect of biofield treatment on structural and morphological properties of silicon carbide. J Powder Metall Min 4: 132. 18. Trivedi MK, Nayak G, Patil S, Tallapragada RM, Latiyal O (2015) Evaluation of biofield treatment on physical, atomic and structural characteristics of manganese (II, III) oxide. J Material Sci Eng 4: 177. 19. Trivedi MK, Nayak G, Patil S, Tallapragada RM, Latiyal O, et al. (2015) An evaluation of biofield treatment on thermal, physical and structural properties of cadmium powder. J Thermodyn Catal 6: 147. 20. Curry JA, Webster PJ (1999) Thermodynamics of atmospheres and ocean. Academic Press Medical. 21. Wiberg E, Wiberg N (2001) Inorganic chemistry. Academic Press. Science. 22. Zong F, Meng C, Guo Z, Ji F, Xiao H (2010) Synthesis and characterization of magnesium nitride powder formed by Mg direct reaction with N2. J Alloy Compd 508 172-176. 23. Kim D, Kim T, Park H, Park D (2011) Synthesis of nanocrystalline magnesium nitride (Mg3N2) powder using thermal plasma Appl Surf Sci 257: 5375-5379. 24. Mei L, Li JT (2009) Combustion synthesis of ultrafine magnesium nitride powder by Ar dilution. Scripta Mater 60: 141-143. 25. Inoue M, Hirasawa I (2013) The relationship between crystal morphology and XRD peak intensity on CaSO4•2H2O. J Cryst Growth 380: 169-175. 26. Hirai H, Kondo T, Hasegawa M, Yagi T, Sakashita M, et al. (2000) Structural changes of methane hydrate under high pressure at room temperature. High pressure (Science). 27. Mohapatra J (2013) Defect-related blue emission from ultra-fine Zn1−xCdxS quantum dots synthesized by simple beaker chemistry. Int Nano Lett 3:31. 28. Paszkowicz W, Knapp M, Domagala JZ, Kamler G, Podsiadlo S (2001) Lowtemperature thermal expansion of Mg3N2. J Alloy Compd 328: 272-275. 29. Soboyejo W (2002) Mechanical properties of engineered materials. CRC press.