Precipitation and Growth of Intermatallic Phases in an Fe-Ni Superalloy during Prolonged Ageing

Article Preview

Abstract:

The influence of prolonged aging on the precipitation process of intermetallic phases, as well as carbide and boride in an Fe-Ni superalloy has been studied. The samples were subjected to a solution heat treatment at 980°C for 2 h and water quenched, and then aged at 715, 750 and 780°C for 0.5-500 h. The samples were analysed using transmission electron microscopy (TEM) and X-ray diffraction. Direct measurements on the electron micrographs allowed to calculate the mean diameter () of the γ’ phase. The growth step of the γ’ phase particles has been analysed on the basis of the LSW theory, as well as the activation energy of the γ’ phase coagulation has been estimated.

You might also be interested in these eBooks

Info:

Periodical:

Solid State Phenomena (Volume 246)

Pages:

29-32

Citation:

Online since:

February 2016

Export:

Price:

* - Corresponding Author

[1] K.J. Ducki, Research of the microstructure and precipitation strengthening in a high-temperature Fe-Ni superalloy, IOP Conference Series – Mater. Sci. Eng. 35 (2012) 012007.

DOI: 10.1088/1757-899x/35/1/012007

Google Scholar

[2] K.J. Ducki, J. Mendala, L. Wojtynek, TEM and X-ray examination of intermetallic phases and carbides precipitation in an Fe-Ni superalloy during prolonged ageing, Solid State Phenom. 212 (2014) 15-20.

DOI: 10.4028/www.scientific.net/ssp.212.15

Google Scholar

[3] L. Pająk, K.J. Ducki, L. Wojtynek, X-ray analysis of the precipitation process in an Fe-Ni superalloy, Solid State Phenom. 212 (2014) 225-228.

DOI: 10.4028/www.scientific.net/ssp.212.225

Google Scholar

[4] I.M. Lifshitz, V.V. Slyozow, The kinetics of the precitipitation from supersaturated solid solution, J. Phys. Chem. Solids 19 (1961) 35-50.

Google Scholar

[5] C. Wagner, Theorie der Alterung von Niederschlägen durch Umlösen (Ostvald Reifung), Z. Elektroch. 65 (1961) 581-591.

DOI: 10.1002/bbpc.19610650704

Google Scholar

[6] J. Szala, Computer Program Met-Ilo for Image Analysis in Material Science, Silesian University of Technology, Materials Science Department, Katowice, (1997).

Google Scholar

[7] A. Czyrska-Filemonowicz, B. Dubiel, K. Wiencek, Determination of the oxide particle density in ODS alloys by means of transmission electron microscopy, Acta Stereol. 17 (1998) 225-236.

Google Scholar

[8] K. Kusabiraki, X. Zhang, T. Ooka, The Growth of γ' Precipitates in a 53Ni-20Co-15Cr Superalloy, ISIJ Int. 35 (1995) 1115-1120.

DOI: 10.2355/isijinternational.35.1115

Google Scholar