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Tales of the Abnormal: Nanocrystalline Grain Growth at Low Temperatures
Abstract:
Employing x-ray diffractometry and electron microscopy, we have investigated thermally induced microstructural evolution in ball-milled nanocrystalline Fe. At low annealing temperatures, the early-stage growth of the area-weighted and volume-weighted average grain sizes deviates strongly from the parabolic behavior expected for normal grain growth. Analysis of the ratio of these two averages indicates that the width of the grain-size distribution changes with time. This result is more consistent with the occurrence of a transient stage of abnormal grain growth than with a grain-size-dependent change in the rate-limiting mechanism for grain-boundary migration.
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315-316
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April 2012
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