Synthesis, Growth and Characterisation of Novel Semiorganic Material: Lithium Boro-Succinate

M. Lakshmipriya; D. Rajan Babu; R. Ezhil Vizhi

doi:10.4028/www.scientific.net/AMR.584.141

Paper Titles

Growth of Ethyl-Para-Hydroxybenzoate Single Crystal and its Characterization
p.121

Hot Corrosion Studies of GTA Welded Monel 400 Exposed to Thin Film of Molten Na₂so₄ - 60% V₂O₅ at 600°C
p.126

Studies on Thin Film Oxide Formation on GTA Welded AISI 304 & AISI 310S Exposed at 600°C
p.131

Crystal Growth, Spectral, Thermal and Optical Properties of Phthalic Anhydride (PA) Single Crystal
p.136

Synthesis, Growth and Characterisation of Novel Semiorganic Material: Lithium Boro-Succinate
p.141

Mechanical Studies of Nonlinear Optical γ-Glycine Single Crystal Grown in the Presence of Lithium Nitrate
p.145

Effect of B₂O₃ Flux on the Crystal Structure, Dielectric Properties of (K _0.5Na_0.5)NbO₃ Single Crystal Grown by Flux Method
p.150

Thermoelectric Property in Multiferroics
p.157

High-Temperature Electrical Transport Property of Misfit Cobaltite of Ca_3-xNd_xCo_4-xCu_xO₉ (x = 0.0 – 0.4)
p.162

HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 584Synthesis, Growth and Characterisation of Novel...

Synthesis, Growth and Characterisation of Novel Semiorganic Material: Lithium Boro-Succinate

Abstract:

Single crystal of lithium boro-succinate (LiBS), a semiorganic nonlinear optical material has been grown by slow evaporation method at ambient temperature. The lattice parameter and crystal structure were analysed by powder XRD. The optical transmission spectra revealed optical properties of the grown crystal. FTIR studies confirm the presence of functional group. TGA/DSC studies were carried to find the melting point of the material. Micro hardness has been estimated from LiBS crystal at different forces and various constants were determined by Vickers hardness test.

You might also be interested in these eBooks

View Preview

Info:

Periodical:

Advanced Materials Research (Volume 584)

Pages:

141-144

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.584.141

Citation:

Cite this paper

Online since:

October 2012

Authors:

M. Lakshmipriya, D. Rajan Babu, R. Ezhil Vizhi

Keywords:

Solution Growth, Thermal Analysis, X-Ray Diffraction (XRD)

Export:

RIS, BibTeX

Price:

Permissions:

Request Permissions

References

[1] G. Anandha Babu, P. Ramasamy , Synthesis, crystal growth and characterization of novel semiorganic nonlinear optical crystal: Dichlorobis(l-proline)zinc(II), Materials Chemistry and Physics 113 (2009) 727–733

DOI: 10.1016/j.matchemphys.2008.08.041

Google Scholar

[2] M. N. Ravishankar, R. Chandramani and A.P. Gnanaprakash, Optical and mechanical characterization of solution grown semi organic nlo crystals , Rasayan J.chem Vol.4, No.1 (2011) 86-90.

Google Scholar

[3] I.Pritula,A. Kosinova, M. Kolybayeva, V. Puzikov, S. Bondarenko, V. Tkachenko, V. Tsurikov, O. Fesenko , Optical, structural and microhardness properties of KDP crystals grown from urea-doped solutions, Materials Research Bulletin Volume 43 (2008) 2778–2789.

DOI: 10.1016/j.materresbull.2007.10.040

Google Scholar

[4] P. Anandan, G.Parthipan, T.Saravanan, R.MohanKumar, G.Bhagavannarayana, R.Jayavel , Crystal growth, structural and optical characterization of a semi-organic single crystal for frequency conversion applications, Physica B 405 (2010) 4951–4956

DOI: 10.1016/j.physb.2010.09.042

Google Scholar

[5] Fernando Loretta, T. Josephine Rani, P. Selvarajan, S. Perumal and S. Ramalingom, Growth, structural and optical studies of pure and bisthiourea zinc chloride doped potassium dihydrogen phosphate single crystals, World Journal of Science and Technology 1(3) 2011 01-06.

DOI: 10.1063/1.3646805

Google Scholar

[6] Keyan Li, Xingtao Wang, Fangfang Zhang, and Dongfeng Xue , Electronegativity Identification of Novel Superhard Materials, Phys. Rev. Lett. 100, (2008) 235-504 .

DOI: 10.1103/physrevlett.100.235504

Google Scholar

[7] M. Senthil Pandian, P. Ramasamy, Conventional slow evaporation and Sankaranarayanan–Ramasamy (SR) method grown diglycine zinc chloride (DGZC) single crystal and its comparative study , Journal of Crystal Growth 312 (2010) 413–419.

DOI: 10.1016/j.jcrysgro.2009.11.011

Google Scholar

[8] V. Chithambaram , S. Jerome Das, R. Arivudai Nambi , S. Krishnan Synthesis, growth and characterization of novel semiorganic nonlinear optical potassium boro-succinate (KBS) single crystals, Optics & Laser Technology 43 (2011) 1229–1232.

DOI: 10.1016/j.optlastec.2011.03.014

Google Scholar