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Determination of 56 Elements in Lake Baikal Water by High-Resolution ICP-MS with the Aid of a Tandem Preconcentration Method

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Abstract

A tandem preconcentration method integrating chelating resin adsorption and La coprecipitation was applied to an analysis of Lake Baikal water by high-resolution ICP-MS. As a result, 56 elements were determined in Lake Baikal water: Ca, Na, Mg, K, Si, Sr, B, Li, Ba, P, Fe, Al, Mo, Zn, Mn, Rb, U, As, V, Cu, Pb, W, Y, Cs, Se, Cr, Ni, Ti, Sb, Zr, Sn, Co, Cd, Rh, Te, Hf, Nb, Ru, Ga, Sc, Th, Bi, and all-rare earth elements (all-REEs), except for Pm. The concentrations of these elements covered a range of nine orders of magnitude, from approximately 17 mg µL–1 of Ca to less than 50 fg µL–1 of Tm. The elemental concentrations in Lake Baikal water were compared with reference data.

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Authors and Affiliations

  1. Department of Applied Chemistry, Graduate School of Engineering, Nagoya University, Furo-cho, Chikusa, Nagoya, 464-8603, Japan

    Dwinna Rahmi, Yanbei Zhu, Tomonari Umemura & Hiroki Haraguchi

  2. Environmental Standard Section, Inorganic Analytical Chemistry Division, National Metrology Institute of Japan (NMIJ), National Institute of Advanced Industrial Science and Technology (AIST), 1–1–1 Umezono, Tsukuba, Ibaraki, 305-8563, Japan

    Yanbei Zhu & Koichi Chiba

  3. College of Education, University of the Ryukyus, Azasenbaru, Nishihara-cho, Okinawa, 903-0213, Japan

    Akihide Itoh

Authors
  1. Dwinna Rahmi
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  2. Yanbei Zhu
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  3. Tomonari Umemura
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  4. Hiroki Haraguchi
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  5. Akihide Itoh
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  6. Koichi Chiba
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Correspondence to Yanbei Zhu.

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Rahmi, D., Zhu, Y., Umemura, T. et al. Determination of 56 Elements in Lake Baikal Water by High-Resolution ICP-MS with the Aid of a Tandem Preconcentration Method. ANAL. SCI. 24, 1513–1517 (2008). https://doi.org/10.2116/analsci.24.1513

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  • DOI: https://doi.org/10.2116/analsci.24.1513

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