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Analysis of Single Synthetic Fibers Using a Portable Total Reflection X-ray Fluorescence Spectrometer

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Abstract

In this study, we developed a simple and one-step Pd separation technique based on photoreduction with Xe lamp irradiation for the determination of 107Pd in highly radioactive samples. A simulated high-level radioactive liquid wastes (HLLW) solution, consisting of 14 major elements in a 3 mol L−1 HNO3 solution, was used to evaluate the separation performance. The Pd precipitate was formed by Xe lamp irradiation, and recovered by centrifugation. The Pd recovery from the simulated HLLW solution reached up to 50%, while 99.5% of the other 13 elements was separated. These results indicate that the applicability of the proposed separation technique to HLLW samples. Keywords Palladium-107, ICP-MS, xenon lamp, photo reduction, precipitation

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Authors and Affiliations

  1. Department of Industrial Chemistry, Tokyo University of Science, 1-3 Kagurazaka, Shinjuku, Tokyo, 162-8601, Japan

    Yawara Sengoku & Shinsuke Kunimura

  2. TOSA Innovative Human Development Programs, Kochi University, 2-5-1 Akebono-cho, Kochi, 780-8520, Japan

    Yoshie Tokuoka & Hibiki Komatsu

  3. Division of Chemistry, Faculty of Education, Kochi University, 2-5-1 Akebono-cho, Kochi, 780-8520, Japan

    Yoshinori Nishiwaki

Authors
  1. Yawara Sengoku
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  2. Yoshie Tokuoka
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  3. Hibiki Komatsu
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  4. Yoshinori Nishiwaki
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  5. Shinsuke Kunimura
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Correspondence to Shinsuke Kunimura.

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Sengoku, Y., Tokuoka, Y., Komatsu, H. et al. Analysis of Single Synthetic Fibers Using a Portable Total Reflection X-ray Fluorescence Spectrometer. ANAL. SCI. 37, 1829–1833 (2021). https://doi.org/10.2116/analsci.21N020

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  • DOI: https://doi.org/10.2116/analsci.21N020

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