Research Article
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Year 2023, Volume: 10 Issue: 2, 277 - 286, 31.05.2023
https://doi.org/10.18596/jotcsa.1097197

Abstract

References

  • 1. Zhu G, Zhang C yang. Functional nucleic acid-based sensors for heavy metal ion assays. Analyst. 2014 Sep 25;139(24):6326–42.
  • 2. Kim HN, Ren WX, Kim JS, Yoon J. Fluorescent and colorimetric sensors for detection of lead, cadmium, and mercury ions. Chem Soc Rev. 2012;41(8):3210–44.
  • 3. Lin YW, Huang CC, Chang HT. Gold nanoparticle probes for the detection of mercury, lead and copper ions. Analyst. 2011;136(5):863–71.
  • 4. Khan H, Jamaluddin Ahmed M, Iqbal Bhanger M. A simple spectrophotometric method for the determination of trace level lead in biological samples in the presence of aqueous micellar solutions. Spectroscopy. 2006;20(5–6):285–97.
  • 5. Clayton GD, Clayton FE. Patty’s industrial hygiene and toxicology. Vol. 2A. Toxicology. John Wiley & Sons, Inc., Baffins Lane, Chichester, Sussex PO19 1DU; 1981. ISBN: 978-0-471-16042-7.
  • 6. Steenland K, Boffetta P. Lead and cancer in humans: Where are we now? Am J Ind Med. 2000 Sep;38(3):295–9.
  • 7. Aragay G, Pons J, Merkoçi A. Recent Trends in Macro-, Micro-, and Nanomaterial-Based Tools and Strategies for Heavy-Metal Detection. Chem Rev. 2011 May 11;111(5):3433–58.
  • 8. Rivas RE, López-García I, Hernández-Córdoba M. Microextraction based on solidification of a floating organic drop followed by electrothermal atomic absorption spectrometry for the determination of ultratraces of lead and cadmium in waters. Anal Methods. 2010;2(3):225.
  • 9. Grindlay G, Mora J, Gras L, de Loos-Vollebregt MTC. Ultratrace determination of Pb, Se and As in wine samples by electrothermal vaporization inductively coupled plasma mass spectrometry. Analytica Chimica Acta. 2009 Oct;652(1–2):154–60.
  • 10. Hsieh HF, Chang WS, Hsieh YK, Wang CF. Lead determination in whole blood by laser ablation coupled with inductively coupled plasma mass spectrometry. Talanta. 2009 Jul 15;79(2):183–8.
  • 11. Miao X, Ling L, Shuai X. Ultrasensitive detection of lead(ii) with DNAzyme and gold nanoparticles probes by using a dynamic light scattering technique. Chem Commun. 2011;47(14):4192.
  • 12. Beqa L, Singh AK, Khan SA, Senapati D, Arumugam SR, Ray PC. Gold Nanoparticle-Based Simple Colorimetric and Ultrasensitive Dynamic Light Scattering Assay for the Selective Detection of Pb(II) from Paints, Plastics, and Water Samples. ACS Appl Mater Interfaces. 2011 Mar 23;3(3):668–73.
  • 13. Nie D, Wu H, Zheng Q, Guo L, Ye P, Hao Y, et al. A sensitive and selective DNAzyme-based flow cytometric method for detecting Pb 2+ ions. Chem Commun. 2012;48(8):1150–2.
  • 14. Wang B, Luo B, Liang M, Wang A, Wang J, Fang Y, et al. Chemical amination of graphene oxides and their extraordinary properties in the detection of lead ions. Nanoscale. 2011;3(12):5059.
  • 15. Lin CH, Wu HL, Huang YL. Combining high-performance liquid chromatography with on-line microdialysis sampling for the simultaneous determination of ascorbyl glucoside, kojic acid, and niacinamide in bleaching cosmetics. Analytica Chimica Acta. 2007 Jan;581(1):102–7.
  • 16. Hou R, Niu X, Cui F. A label-free biosensor for selective detection of DNA and Pb 2+ based on a G-quadruplex. RSC Adv. 2016;6(10):7765–71.
  • 17. Zhao XH, Kong RM, Zhang XB, Meng HM, Liu WN, Tan W, et al. Graphene–DNAzyme Based Biosensor for Amplified Fluorescence “Turn-On” Detection of Pb 2+ with a High Selectivity. Anal Chem. 2011 Jul 1;83(13):5062–6.
  • 18. Wang X, Guo X. Ultrasensitive Pb2+ detection based on fluorescence resonance energy transfer (FRET) between quantum dots and gold nanoparticles. Analyst. 2009;134(7):1348.
  • 19. Hu ZQ, Lin C sheng, Wang XM, Ding L, Cui CL, Liu SF, et al. Highly sensitive and selective turn-on fluorescent chemosensor for Pb2+ and Hg2+ based on a rhodamine–phenylurea conjugate. Chem Commun. 2010;46(21):3765.
  • 20. Li T, Dong S, Wang E. A Lead(II)-Driven DNA Molecular Device for Turn-On Fluorescence Detection of Lead(II) Ion with High Selectivity and Sensitivity. J Am Chem Soc. 2010 Sep 29;132(38):13156–7.
  • 21. Wu J, Qin Y. Polymeric optodes based on upconverting nanorods for fluorescence measurements of Pb2+ in complex samples. Sensors and Actuators B: Chemical. 2014 Mar;192:51–5.
  • 22. Tümay SO, Şanko V, Şenocak A, Demirbas E. A hybrid nanosensor based on novel fluorescent iron oxide nanoparticles for highly selective determination of Hg 2+ ions in environmental samples. New J Chem. 2021;45(32):14495–507.
  • 23. Ge L, Liu H. Engineering Grey Nanosystem as Activatable Ratio-colorimetric Probe for Detection of Lead Ions in Preserved Egg. ANAL SCI. 2020 Nov;36(11):1407–13.
  • 24. Elbaz J, Shlyahovsky B, Willner I. A DNAzyme cascade for the amplified detection of Pb2+ ions or l-histidine. Chem Commun. 2008;(13):1569.
  • 25. Liu XH, Zheng H, Zhong L, Huang S, Karki K, Zhang LQ, et al. Anisotropic Swelling and Fracture of Silicon Nanowires during Lithiation. Nano Lett. 2011 Aug 10;11(8):3312–8.
  • 26. Reese CE, Asher SA. Photonic Crystal Optrode Sensor for Detection of Pb 2+ in High Ionic Strength Environments. Anal Chem. 2003 Aug 1;75(15):3915–8.
  • 27. Hamid A, Aamer S, Farukh J, Abdul B, Irfan ZQ, Abdul A, et al. Synthesis, Characterization, Biological and Docking Simulations of 4-(Benzylideneamino) Benzoic Acids ((1)). CHINESE JOURNAL OF STRUCTURAL CHEMISTRY. 2021;40(3):291–300.
  • 28. Valarmathy G, Subbalakshmi R, Sabarika B, Nisha C. Schiff bases derived from 4-amino-N-substituted benzenesulfonamide: synthesis, spectral characterisation and MIC evaluation. Bull Chem Soc Eth. 2021 Oct 24;35(2):435–48.
  • 29. Ferroudj N, Nzimoto J, Davidson A, Talbot D, Briot E, Dupuis V, et al. Maghemite nanoparticles and maghemite/silica nanocomposite microspheres as magnetic Fenton catalysts for the removal of water pollutants. Applied Catalysis B: Environmental. 2013 Jun;136–137:9–18.
  • 30. Shah K, Hassan E, Ahmed F, Anis I, Rabnawaz M, Shah MR. Novel fluorene-based supramolecular sensor for selective detection of amoxicillin in water and blood. Ecotoxicology and Environmental Safety. 2017 Jul;141:25–9.

Synthesis of Imino Stabilized Iron Oxide Nanosensor for Selective Detection of Lead Ions

Year 2023, Volume: 10 Issue: 2, 277 - 286, 31.05.2023
https://doi.org/10.18596/jotcsa.1097197

Abstract

The present work describes the successful preparation of iron oxide nanoparticles (NSB1) stabilized with 4-((2-hydroxybenzylidene)amino)benzoic acid. The characterization has been achieved through ultraviolet visible (UV-Vis), fourier transform infra-red (FTIR) spectroscopy and scanning electron microscopy (SEM) with electron dispersive X-ray elemental analysis (EDX). These magnetic nanoparticles have exhibited significant chemosensing properties in the aqueous media to screen Cr3+, Cd2+, Li+, Co2+, Al3+, Pb2+, Ni2+ and Sr2+ ions. However, lead (Pb2+) ions have shown the highest selectivity as compared to other metal ions without any interference in the competitive ion study. The detection limit of Pb2+ ions was found to be 1.7 µM by this nanosensor. The binding ratio and stoichiometry was found to be 1:1 as measured by Job’s plot. The binding strength was also computed through Benesei-Hildebrand equation.

References

  • 1. Zhu G, Zhang C yang. Functional nucleic acid-based sensors for heavy metal ion assays. Analyst. 2014 Sep 25;139(24):6326–42.
  • 2. Kim HN, Ren WX, Kim JS, Yoon J. Fluorescent and colorimetric sensors for detection of lead, cadmium, and mercury ions. Chem Soc Rev. 2012;41(8):3210–44.
  • 3. Lin YW, Huang CC, Chang HT. Gold nanoparticle probes for the detection of mercury, lead and copper ions. Analyst. 2011;136(5):863–71.
  • 4. Khan H, Jamaluddin Ahmed M, Iqbal Bhanger M. A simple spectrophotometric method for the determination of trace level lead in biological samples in the presence of aqueous micellar solutions. Spectroscopy. 2006;20(5–6):285–97.
  • 5. Clayton GD, Clayton FE. Patty’s industrial hygiene and toxicology. Vol. 2A. Toxicology. John Wiley & Sons, Inc., Baffins Lane, Chichester, Sussex PO19 1DU; 1981. ISBN: 978-0-471-16042-7.
  • 6. Steenland K, Boffetta P. Lead and cancer in humans: Where are we now? Am J Ind Med. 2000 Sep;38(3):295–9.
  • 7. Aragay G, Pons J, Merkoçi A. Recent Trends in Macro-, Micro-, and Nanomaterial-Based Tools and Strategies for Heavy-Metal Detection. Chem Rev. 2011 May 11;111(5):3433–58.
  • 8. Rivas RE, López-García I, Hernández-Córdoba M. Microextraction based on solidification of a floating organic drop followed by electrothermal atomic absorption spectrometry for the determination of ultratraces of lead and cadmium in waters. Anal Methods. 2010;2(3):225.
  • 9. Grindlay G, Mora J, Gras L, de Loos-Vollebregt MTC. Ultratrace determination of Pb, Se and As in wine samples by electrothermal vaporization inductively coupled plasma mass spectrometry. Analytica Chimica Acta. 2009 Oct;652(1–2):154–60.
  • 10. Hsieh HF, Chang WS, Hsieh YK, Wang CF. Lead determination in whole blood by laser ablation coupled with inductively coupled plasma mass spectrometry. Talanta. 2009 Jul 15;79(2):183–8.
  • 11. Miao X, Ling L, Shuai X. Ultrasensitive detection of lead(ii) with DNAzyme and gold nanoparticles probes by using a dynamic light scattering technique. Chem Commun. 2011;47(14):4192.
  • 12. Beqa L, Singh AK, Khan SA, Senapati D, Arumugam SR, Ray PC. Gold Nanoparticle-Based Simple Colorimetric and Ultrasensitive Dynamic Light Scattering Assay for the Selective Detection of Pb(II) from Paints, Plastics, and Water Samples. ACS Appl Mater Interfaces. 2011 Mar 23;3(3):668–73.
  • 13. Nie D, Wu H, Zheng Q, Guo L, Ye P, Hao Y, et al. A sensitive and selective DNAzyme-based flow cytometric method for detecting Pb 2+ ions. Chem Commun. 2012;48(8):1150–2.
  • 14. Wang B, Luo B, Liang M, Wang A, Wang J, Fang Y, et al. Chemical amination of graphene oxides and their extraordinary properties in the detection of lead ions. Nanoscale. 2011;3(12):5059.
  • 15. Lin CH, Wu HL, Huang YL. Combining high-performance liquid chromatography with on-line microdialysis sampling for the simultaneous determination of ascorbyl glucoside, kojic acid, and niacinamide in bleaching cosmetics. Analytica Chimica Acta. 2007 Jan;581(1):102–7.
  • 16. Hou R, Niu X, Cui F. A label-free biosensor for selective detection of DNA and Pb 2+ based on a G-quadruplex. RSC Adv. 2016;6(10):7765–71.
  • 17. Zhao XH, Kong RM, Zhang XB, Meng HM, Liu WN, Tan W, et al. Graphene–DNAzyme Based Biosensor for Amplified Fluorescence “Turn-On” Detection of Pb 2+ with a High Selectivity. Anal Chem. 2011 Jul 1;83(13):5062–6.
  • 18. Wang X, Guo X. Ultrasensitive Pb2+ detection based on fluorescence resonance energy transfer (FRET) between quantum dots and gold nanoparticles. Analyst. 2009;134(7):1348.
  • 19. Hu ZQ, Lin C sheng, Wang XM, Ding L, Cui CL, Liu SF, et al. Highly sensitive and selective turn-on fluorescent chemosensor for Pb2+ and Hg2+ based on a rhodamine–phenylurea conjugate. Chem Commun. 2010;46(21):3765.
  • 20. Li T, Dong S, Wang E. A Lead(II)-Driven DNA Molecular Device for Turn-On Fluorescence Detection of Lead(II) Ion with High Selectivity and Sensitivity. J Am Chem Soc. 2010 Sep 29;132(38):13156–7.
  • 21. Wu J, Qin Y. Polymeric optodes based on upconverting nanorods for fluorescence measurements of Pb2+ in complex samples. Sensors and Actuators B: Chemical. 2014 Mar;192:51–5.
  • 22. Tümay SO, Şanko V, Şenocak A, Demirbas E. A hybrid nanosensor based on novel fluorescent iron oxide nanoparticles for highly selective determination of Hg 2+ ions in environmental samples. New J Chem. 2021;45(32):14495–507.
  • 23. Ge L, Liu H. Engineering Grey Nanosystem as Activatable Ratio-colorimetric Probe for Detection of Lead Ions in Preserved Egg. ANAL SCI. 2020 Nov;36(11):1407–13.
  • 24. Elbaz J, Shlyahovsky B, Willner I. A DNAzyme cascade for the amplified detection of Pb2+ ions or l-histidine. Chem Commun. 2008;(13):1569.
  • 25. Liu XH, Zheng H, Zhong L, Huang S, Karki K, Zhang LQ, et al. Anisotropic Swelling and Fracture of Silicon Nanowires during Lithiation. Nano Lett. 2011 Aug 10;11(8):3312–8.
  • 26. Reese CE, Asher SA. Photonic Crystal Optrode Sensor for Detection of Pb 2+ in High Ionic Strength Environments. Anal Chem. 2003 Aug 1;75(15):3915–8.
  • 27. Hamid A, Aamer S, Farukh J, Abdul B, Irfan ZQ, Abdul A, et al. Synthesis, Characterization, Biological and Docking Simulations of 4-(Benzylideneamino) Benzoic Acids ((1)). CHINESE JOURNAL OF STRUCTURAL CHEMISTRY. 2021;40(3):291–300.
  • 28. Valarmathy G, Subbalakshmi R, Sabarika B, Nisha C. Schiff bases derived from 4-amino-N-substituted benzenesulfonamide: synthesis, spectral characterisation and MIC evaluation. Bull Chem Soc Eth. 2021 Oct 24;35(2):435–48.
  • 29. Ferroudj N, Nzimoto J, Davidson A, Talbot D, Briot E, Dupuis V, et al. Maghemite nanoparticles and maghemite/silica nanocomposite microspheres as magnetic Fenton catalysts for the removal of water pollutants. Applied Catalysis B: Environmental. 2013 Jun;136–137:9–18.
  • 30. Shah K, Hassan E, Ahmed F, Anis I, Rabnawaz M, Shah MR. Novel fluorene-based supramolecular sensor for selective detection of amoxicillin in water and blood. Ecotoxicology and Environmental Safety. 2017 Jul;141:25–9.
There are 30 citations in total.

Details

Primary Language English
Journal Section RESEARCH ARTICLES
Authors

Erum Hasan 0000-0002-2175-4798

Syed Alı 0000-0003-3459-1497

Ambreen Zia 0000-0002-9651-0894

Sabira Begum 0000-0002-1173-2413

Salman Tariq Khan 0000-0002-4916-9136

Syeda Bukhari 0000-0002-5940-0506

Publication Date May 31, 2023
Submission Date April 18, 2022
Acceptance Date January 26, 2023
Published in Issue Year 2023 Volume: 10 Issue: 2

Cite

Vancouver Hasan E, Alı S, Zia A, Begum S, Khan ST, Bukhari S. Synthesis of Imino Stabilized Iron Oxide Nanosensor for Selective Detection of Lead Ions. JOTCSA. 2023;10(2):277-86.