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IR Reflectivity Studies of Mechanically Alloyed PbTe Nanocrystals

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Abstract

Nano-crystalline lead telluride powder was synthesized by mechanical alloying using a high-energy planetary ball mill. The broadening of the X-ray diffraction peaks vs ball milling time, indicates small crystalline size of the order of 30nm. IR spectroscopy results are discussed and compared to the material prepared from melt.

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References

  1. Thermoelectrics Handbook: Macro to Nano, (2006) Ed: D. M. Rowe, CRC Press

  2. M.S. Dresselhaus, G. Chen, M.Y. Tang, R. Yang, H. Lee, D.Z. Wang, Z.F. Ren, J.P. Fleurial, and P. Gogna, (2007) New Directions for Low-Dimensional Thermoelectric Materials, Advanced Materials, 19, 1043–1053.

    CAS  Google Scholar 

  3. N. Bouad, R.M. Marin-Ayral, G. Nabiasa, J.C. Tedenac, (2002). Phase transformation study of Pb–Te powders during mechanical alloying, J. All.Comp. 353, 184–188

    Google Scholar 

  4. J.I Langford, A.J.C Wilson, (1978) Scherrer after 60 years: A Survey and some new Results in the Determination of Crystalline Size, J. Appl. Cryst. 11, 102 –112

    CAS  Google Scholar 

  5. J.R. Dixon and H.R. Riedl , (1965) Electric-Susceptibility Hole Mass of Lead Telluride Phys. Rev. 138, A873–A881

    Google Scholar 

  6. H. R. Riedl, J. R. Dixon and R. B. Schoolar, (1967) Reflectivity of Tin Telluride in the Infrared Phys. Rev. 162, 692–700

    CAS  Google Scholar 

  7. H.R. Riedl, Free-Carrier Absorption in p-type PbTe, Phys. Rev., 127, 162 (1962)

    CAS  Google Scholar 

  8. A. A. Kukharskii, (1973) Plasmon-Phonon Coupling in GaAs Solid State Communications, 13, 1761–1765

    Article  CAS  Google Scholar 

  9. P. Beckman and A. Spizzichino, (1963) The scattering of electromagnetic waves from rough surfaces, Pergamon Press, Oxford

    Google Scholar 

  10. D.A.G. Bruggeman, (1935) Berechnung verschiedener physikalischer Konstantenvon heterogenen Substanzen, Ann. Phys. (Leipzig) 24, 636–679

    Google Scholar 

  11. (a) Landolt-Börnstein, III/41: Semiconductors –Subvolume III/41C: Non-tetrahedrally Bonded Elements and Binary Compounds I, Springer Series in Solid State Sciences (b) Schlicht, B., Dornhaus, K., Nimtz, G., Haas, L. D., Jakobus, T.: Solid State Electron. 21 (1978) 1481.

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Hasapis, T., Papageorgiou, C., Hatzikraniotis, E. et al. IR Reflectivity Studies of Mechanically Alloyed PbTe Nanocrystals. MRS Online Proceedings Library 1166, 312 (2009). https://doi.org/10.1557/PROC-1166-N03-12

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  • DOI: https://doi.org/10.1557/PROC-1166-N03-12

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