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Characterization of superdislocation dissociations in Al66Ti25Cr9 with transmission electron microscopy observations and image simulations

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Abstract

The nature of dissociated superlattice dislocation cores in Al66Ti25Cr9, deformed at room temperature, has been characterized by weak-beam transmission electron microscopy (TEM) and comparison of experimental images with computer-simulated images. The displacement fields associated with narrowly dissociated APB- and SISF-dissociated ‹110› superdislocations were calculated to account for the asymmetry in dislocation contrast and led to a better understanding of the formation of images. Such calculations are a powerful aid, when coupled with image simulations, in distinguishing the “real” intensity peaks from the supplementary peaks that can be generated under experimental imaging conditions. While both APB- and SISF-dissociated superdislocations were identified, the vast majority of superdislocations were determined to be APB-dissociated. Corrected values of the fault energies (γAPB and γSISF ) have been measured for this alloy. These energies and the observed dissociations are shown to be self-consistent.

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References

  1. Dislocations in Solids, edited by F. R. N. Nabarro and M. S. Duesbery (North-Holland, Amsterdam, 1996), Vol. 10.

    Google Scholar 

  2. M. Yamaguchi, V. Paidar, D. P. Pope, and V. Vitek, Philos. Mag. A 45, 867 (1982).

    Article  CAS  Google Scholar 

  3. V. Paidar, M. Yamaguchi, D. P. Pope, and V. Vitek, Philos. Mag. A 45, 883 (1982).

    Article  CAS  Google Scholar 

  4. K. S. Kumar, Int. Metals Rev. 35, 293 (1990).

    Article  Google Scholar 

  5. V. K. Vasudevan, R. Wheeler, and H. L. Fraser, in High Temperature Ordered Intermetallic Alloys III, edited by C. T. Liu, A. I. Taub, N. S. Stoloff, and C. C. Koch (Mater. Res. Soc. Symp. Proc. 133, Pittsburgh, PA, 1989), p. 705.

  6. C. D. Turner, W. O. Powers, and J. A. Wert, Acta Metall. 37, 2635 (1989).

    Article  CAS  Google Scholar 

  7. W. O. Powers and J. A. Wert, Metall. Trans. A 21, 145 (1990).

    Article  Google Scholar 

  8. E. P. George, J. A. Horton, W. D. Porter, and J. H. Schneibel, J. Mater. Res. 5, 1639 (1990).

    Article  CAS  Google Scholar 

  9. G. Hu, S. Chen, X. Wu, and X. Chen, J. Mater. Res. 6, 957 (1991).

    Article  CAS  Google Scholar 

  10. D. G. Morris and R. Lerf, Acta Metall. Mater. 39, 2419 (1991).

    Article  Google Scholar 

  11. D. G. Morris, J. Mater. Res. 7, 303 (1992).

    Article  CAS  Google Scholar 

  12. H. Inui, D. E. Luzzi, W. D. Porter, D. P. Pope, V. Vitek, and M. Yamaguchi, Philos. Mag. A 65, 245 (1992).

    Article  CAS  Google Scholar 

  13. S. Zhang, W. W. Milligan, and D. E. Mikkola, Scripta Metall. Mater. 27, 1073 (1992); Philos. Mag. A 71, 523 (1995).

    Article  CAS  Google Scholar 

  14. X. Wu, Y. Rong, S. Chen, and G. Hu, Scripta Metall. Mater. 28, 1519 (1993).

    Article  CAS  Google Scholar 

  15. Z. L. Wu, D. P. Pope, and V. Vitek, Philos. Mag. A 70, 159 (1994); ibid., 70, p. 171 (1994).

    Article  Google Scholar 

  16. D. G. Morris, R. Lerf, and M. Leboeuf, Acta Metall. Mater. 43, 2825 (1995).

    Article  CAS  Google Scholar 

  17. J. W. Edington, Practical Electron Microscopy in Materials Science (Van Nostrand, New York, 1976).

    Google Scholar 

  18. P. Veyssière and D. G. Morris, Philos. Mag. A 67, 491 (1993).

    Article  Google Scholar 

  19. M. Wilkens and E. Hornbogen, Phys. Status Solidi 4, 557 (1964).

    Article  CAS  Google Scholar 

  20. D. J. H. Cockayne, I. L. F. Ray, and M. J. Whelan, Philos. Mag. A 20, 1265 (1969).

    Article  CAS  Google Scholar 

  21. G. Hug, A. Loiseau, and P. Veyssière, Philos. Mag. A 57, 499 (1988).

    Article  CAS  Google Scholar 

  22. A. Korner, Philos. Mag. A 58, 507 (1988).

    Article  CAS  Google Scholar 

  23. N. Baluc, H. P. Karnthaler, and M. J. Mills, Philos. Mag. A 64, 137 (1991).

    Article  CAS  Google Scholar 

  24. P. Veyssière, ISIJ Int. 31, 1028 (1991).

    Article  Google Scholar 

  25. W. M. Stobbs and C. H. Sworn, Philos. Mag. 24, 1365 (1971).

    Article  CAS  Google Scholar 

  26. C. J. Humphreys, R. A. Drummond, A. Hart-Davis, and E. P. Butler, Philos. Mag. 35, 1543 (1977).

    Article  CAS  Google Scholar 

  27. K. J. Hemker and M. J. Mills, Philos. Mag. A 68, 305 (1993).

    Article  CAS  Google Scholar 

  28. N. Baluc and R. Schäublin, Philos. Mag. A 74, 113 (1996).

    Article  CAS  Google Scholar 

  29. K. J. Hemker, Philos. Mag. A 76 (1) (1997).

  30. R. Schäublin and P. Stadelmann, Mater. Sci. Eng. A164, 373 (1993).

    Article  Google Scholar 

  31. A. K. Head, P. Humble, L. M. Clarebrough, A. J. Morton, and G. T. Forwood, Computed Electron Micrographs and Defect Identification (North-Holland, Amsterdam, 1973).

    Google Scholar 

  32. P. B. Hirsch, A. Howie, R. B. Nicholson, D. W. Pashley, and M. J. Whelan, Electron Microscopy of Thin Crystals (Butterworths, London, 1965).

    Google Scholar 

  33. R. Schäublin, X. Meng, and W. M. Stobbs, Inst. Phys. Conf. Ser. 147, 91 (1995).

    Google Scholar 

  34. P. Stadelmann, Ultramicroscopy 21, 131 (1987).

    Article  CAS  Google Scholar 

  35. A. Weickenmeier and H. Kohl, Acta Crystallogr. A 47, 590 (1991).

    Article  Google Scholar 

  36. D. J. H. Cockayne, Z. Natur. A27, 452 (1972).

    Article  CAS  Google Scholar 

  37. A. N. Stroh, Philos. Mag. 3, 625 (1958).

    Article  CAS  Google Scholar 

  38. N. Baluc, R. Schäublin, and K. J. Hemker, Philos. Mag. Lett. 64, 327 (1991).

    Article  CAS  Google Scholar 

  39. V. Paidar, D. P. Pope, and M. Yamaguchi, Scripta Metall. 15, 1029 (1981).

    Article  CAS  Google Scholar 

  40. D. G. Morris, Scripta Metall. 25, 713 (1991); 26, 733 (1992).

    Article  CAS  Google Scholar 

  41. M. H. Yoo and C. L. Fu, ISIJ Int. 31, 1049 (1991).

    Article  CAS  Google Scholar 

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Kumar, M., Hemker, K.J. Characterization of superdislocation dissociations in Al66Ti25Cr9 with transmission electron microscopy observations and image simulations. Journal of Materials Research 13, 610–624 (1998). https://doi.org/10.1557/JMR.1998.0078

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  • DOI: https://doi.org/10.1557/JMR.1998.0078

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