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Licensed Unlicensed Requires Authentication Published by De Gruyter (O) July 28, 2010

The crystal structure of phenyl hydrazine, C6H5 · NH · NH2

Abstract

X-ray diffraction data from phenyl hydrazine were collected on a Weissenberg Unicam S-35 adapted to low-temperature crystallography by Singh and Ramaseshan. The crystal belongs to the space group P21/c, with unit-cell dimensions a = 9.59 Å, b = 5.91 Å, c = 12.31 Å and β = 118° and four molecular units per cell.

The structure was solved in the (010) projection and the y coordinates were obtained from packing considerations. The R factor for the 385 observed and 300 unobserved reflections in the CuK sphere is 0.16. The N–N bond is off the plane of the remaining atoms of the molecule.

Published Online: 2010-7-28
Published in Print: 1968-10-1

© 2015 Oldenbourg Wissenschaftsverlag GmbH, Rosenheimer Str. 145, 81671 München

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