Synthetic Studies on Nephritogenic Glycosides. Synthesis of α-Glc-(1→6)-β-Glc-(1→6)-α-Glc-(1→Asn)

Tomoya OGAWA; Satoru NAKABAYASHI; Seiichi SHIBATA

doi:10.1271/bbb1961.47.1213

Agricultural and Biological Chemistry

Online ISSN : 1881-1280
Print ISSN : 0002-1369
ISSN-L : 0002-1369

Synthetic Studies on Nephritogenic Glycosides. Synthesis of α-Glc-(1→6)-β-Glc-(1→6)-α-Glc-(1→Asn)

Tomoya OGAWA, Satoru NAKABAYASHI, Seiichi SHIBATA

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JOURNAL FREE ACCESS

1983 Volume 47 Issue 6 Pages 1213-1218

DOI https://doi.org/10.1271/bbb1961.47.1213

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Abstract

Glucotriosyl asparagine 2, a proposed structure for the glycan part of nephritogenic glycopeptide 1 isolated from the glomerular basement-membrane of rat, was synthesized in regioand stereo-selective manners starting from a-D-glucopyranosyl azide 8. The key intermediate for this synthesis was designed to be glucotriosyl azide 21, based on retrosynthetic considerations.

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