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Powder Preparation in Aerosol Deposition Method for Lead Zirconate Titanate Thick Films

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Copyright (c) 2002 The Japan Society of Applied Physics
, , Citation Jun Akedo and Maxim Lebedev 2002 Jpn. J. Appl. Phys. 41 6980 DOI 10.1143/JJAP.41.6980

1347-4065/41/11S/6980

Abstract

The influence of a pre-process for a starting powder in the deposition of ferroelectric thick films using the aerosol deposition method (ADM) was investigated. When a dry-milling procedure was introduced to the preparation of the ferroelectric powder, the deposition rate of ADM increased significantly up to 30-fold and reached 73 µm/min for a 5 mm2 area. However, density and electrical properties of the thick film decreased. If heat treatment at 800°C for 4 h was additionally introduced to the pre-process of the starting powder, the deposition rate increased up to 7–10-fold as compared with that for a starting powder and the electrical properties were improved from Pr=20 µC/cm2 at Ec=50 kV/cm to 32 µC/cm2 at Ec=45 kV/cm.

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10.1143/JJAP.41.6980