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Preparation and Evaluation of Ammonium-Succinic Salts as Shale Swelling Inhibitor and Its Application in Water-Based Drilling Fluids

  • CHEMICAL PHYSICS OF POLYMER MATERIALS
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Abstract

A series of ammonium-succinic salts (ASS) was prepared from succinic acid and amines as small molecule shale swelling inhibitor. It was evaluated by bentonite linear expansion test, anti-swelling experiments. And then the best one, ASS-8 (synthesize with succinic acid and tetraethylenepentamine with the ratio of acid group to amine group 1 : 2), was evaluated in water-based drilling fluid. Anti-swelling results shows that ASS-8 can decrease the swelling volume of bentonite by 90.9% with the concentration of 0.8%. Drilling fluid evaluation sho wed ASS-8 has high inhibitive capability to bentonite hydration swelling in the water-based drilling fluid, and it is compatible with heteropolysaccharide(KD-03) and modified starch. The inhibition mechanism of ASS-8 was studied by thermogravimetric analysis and particle distribution test. These results demonstrate ASS-8 may enter the clay layer and bond the clay sheets together by electrostatic adsorption and hydrogen bonds.

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ACKNOWLEDGMENTS

We are grateful to the Modern Analysis and Testing Center of Xi`an Shiyou University.

Funding

The work was supported financially by National Science and Technology Major Project (no. 2017ZX05069004), Shaanxi Provincial Key Research and Development Program (no. 2019ZDLGY06-03) and Youth Innovation Team of Shaanxi University.

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Authors and Affiliations

  1. Shaanxi Province Key Laboratory of Environmental Pollution Control and Reservoir Protection Technology of Oilfields, Xi’an Shiyou University, 710065, Xi’an, China

    Yuntian Jing,  Jie Zhang, Weimin Hu, Weichao Du, Juan Xie, Chengtun Qu & Gang Chen

  2. Xi’an Key Laboratory of Tight oil (Shale oil) Development (Xi’an Shiyou University), 710065, Xi’an, Shaanxi, China

    Juan Xie & Gang Chen

  3. State Key Laboratory of Petroleum Pollution Control, CNPC Research Institute of Safety and Environmental Technology, 102206, Beijing, China

    Chengtun Qu

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  1. Yuntian Jing
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  2. Jie Zhang
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  3. Weimin Hu
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  4. Weichao Du
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  5. Juan Xie
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  7. Gang Chen
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Correspondence to Chengtun Qu or Gang Chen.

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Yuntian Jing, Jie Zhang, Hu, W. et al. Preparation and Evaluation of Ammonium-Succinic Salts as Shale Swelling Inhibitor and Its Application in Water-Based Drilling Fluids. Russ. J. Phys. Chem. B 15 (Suppl 1), S102–S108 (2021). https://doi.org/10.1134/S1990793121090165

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  • DOI: https://doi.org/10.1134/S1990793121090165

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