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In Situ Preparation of Polymer Nanocomposites Based on Sols of Surface-Modified Detonation Nanodiamonds by Classical and Controlled Radical Polymerization

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Abstract—

The possibility of surface modification of detonation nanodiamonds to give them dispersability in methyl methacrylate is considered. In situ polymer composites are obtained by classical radical polymerization and reversible chain-transfer polymerization based on stable sols of detonation nanodiamonds in a monomer. Evidence that nanodiamonds are dispersed in a polymer matrix up to a size of units of nanometers is given. The effect of detonation nanodiamonds on the molecular weight characteristics and glass transition temperature of poly(methyl metacrylate) obtained in their presence is studied.

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ACKNOWLEDGMENTS

The authors are grateful to V.Yu. Dolmatov (SKTB Technolog) for kindly furnishing the DND sample.

Funding

The small-angle X-ray scattering and differential scanning calorimetry studies were performed using the equipment of the Engineering Center at the St. Petersburg State Institute of Technology (Technical University).

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Authors and Affiliations

  1. St. Petersburg State Institute of Technology (Technical University), 190013, St. Petersburg, Russia

    E. V. Sivtsov & A. I. Gostev

  2. Lebedev Research Institute of Synthetic Rubber, 198035, St. Petersburg, Russia

    A. V. Kalinin, L. V. Agibalova & F. A. Shumilov

  3. ITMO University, 197101, St. Petersburg, Russia

    A. V. Smirnov

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  1. E. V. Sivtsov
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  2. A. V. Kalinin
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  3. A. I. Gostev
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  4. A. V. Smirnov
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  5. L. V. Agibalova
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  6. F. A. Shumilov
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Correspondence to E. V. Sivtsov.

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Translated by K. Utegenov

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Sivtsov, E.V., Kalinin, A.V., Gostev, A.I. et al. In Situ Preparation of Polymer Nanocomposites Based on Sols of Surface-Modified Detonation Nanodiamonds by Classical and Controlled Radical Polymerization. Polym. Sci. Ser. B 62, 734–749 (2020). https://doi.org/10.1134/S1560090420050139

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