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The formation of layers of porous crystalline tin dioxide from a composite on the basis of multiwalled carbon-nanotube arrays

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Abstract

A new method for the synthesis of porous crystalline tin-dioxide (SnO2) layers from composites on the basis of multiwalled carbon nanotubes (MWCNTs) and nonstoichiometric amorphous tin oxide (MWCNT/SnO x ) is proposed. An MWCN/SnO x composite layer produced by magnetron sputtering is annealed in air atmosphere at 500°C for 30 min. A homogeneous porous layer comprised of crystalline SnO2 spherical particles with a size of about 0.1 μm is obtained as a result. In the process of annealing, nearly all the amount of carbon is removed in the form of gaseous oxides (only a small amount remains in the upper part of the porous SnO2 layer). The structural defectiveness of nanotube walls, which increases because of the magnetron deposition of tin, plays a crucial role in the carbon oxidation and destruction of MWCNTs.

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Authors and Affiliations

  1. Omsk Scientific Center, Siberian Branch, Russian Academy of Sciences, Omsk, 644024, Russia

    S. N. Nesov, P. M. Korusenko, V. V. Bolotov, S. N. Povoroznyuk & K. E. Ivlev

  2. St. Petersburg State University, St. Petersburg, 199034, Russia

    D. A. Smirnov

  3. Institute of Solid State Physics, Dresden University of Technology, Dresden, Germany

    D. A. Smirnov

  4. Omsk State Technical University, Omsk, 644050, Russia

    S. N. Povoroznyuk

Authors
  1. S. N. Nesov
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  2. P. M. Korusenko
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  3. V. V. Bolotov
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  4. S. N. Povoroznyuk
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  5. K. E. Ivlev
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  6. D. A. Smirnov
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Corresponding author

Correspondence to S. N. Nesov.

Additional information

Original Russian Text © S.N. Nesov, P.M. Korusenko, V.V. Bolotov, S.N. Povoroznyuk, K.E. Ivlev, D.A. Smirnov, 2017, published in Pis’ma v Zhurnal Tekhnicheskoi Fiziki, 2017, Vol. 43, No. 21, pp. 16–23.

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Nesov, S.N., Korusenko, P.M., Bolotov, V.V. et al. The formation of layers of porous crystalline tin dioxide from a composite on the basis of multiwalled carbon-nanotube arrays. Tech. Phys. Lett. 43, 961–964 (2017). https://doi.org/10.1134/S1063785017110074

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  • DOI: https://doi.org/10.1134/S1063785017110074

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