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Structural Characterization of Triterpene Saponins from Manchurian Aralia by High Resolution Liquid Chromatography–Mass Spectrometry

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Abstract

The mass-spectrometric characteristics of triterpene saponins from Manchurian aralia were studied using high-performance liquid chromatography in combination with high-resolution mass-spectrometric detection. Conditions for the preparation of extracts for the determination of triterpene saponin concentrations in plant raw materials were optimized. The experimental mass-spectrometric characteristics of triterpene saponins were compared with those described in the literature, and the structural formulas of test compounds were proposed.

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Authors and Affiliations

  1. Signal Research Center, 107014, Moscow, Russia

    M. Yu. Sinitsyn, A. V. Aksenov, M. V. Taranchenko & A. M. Antokhin

  2. Faculty of Chemistry, Moscow State University, 119991, Moscow, Russia

    I. A. Rodin, A. N. Stavrianidi & O. A. Shpigun

Authors
  1. M. Yu. Sinitsyn
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  2. A. V. Aksenov
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  3. M. V. Taranchenko
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  4. I. A. Rodin
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  5. A. N. Stavrianidi
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  6. A. M. Antokhin
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  7. O. A. Shpigun
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Correspondence to M. Yu. Sinitsyn.

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Translated by V. Makhlyarchuk

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Sinitsyn, M.Y., Aksenov, A.V., Taranchenko, M.V. et al. Structural Characterization of Triterpene Saponins from Manchurian Aralia by High Resolution Liquid Chromatography–Mass Spectrometry. J Anal Chem 74, 1113–1121 (2019). https://doi.org/10.1134/S1061934819110108

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  • DOI: https://doi.org/10.1134/S1061934819110108

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