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Mapping of local lattice parameter ratios by projective Kikuchi pattern matching

Aimo Winkelmann, Gert Nolze, Grzegorz Cios, and Tomasz Tokarski
Phys. Rev. Materials 2, 123803 – Published 28 December 2018

Abstract

We describe a lattice-based crystallographic approximation for the analysis of distorted crystal structures via electron backscatter diffraction (EBSD) in the scanning electron microscope. EBSD patterns are closely linked to local lattice parameter ratios via Kikuchi bands that indicate geometrical lattice plane projections. Based on the transformation properties of points and lines in the real projective plane, we can obtain continuous estimations of the local lattice distortion based on projectively transformed Kikuchi diffraction simulations for a reference structure. By quantitative image matching to a projective transformation model of the lattice distortion in the full solid angle of possible scattering directions, we enforce a crystallographically consistent approximation in the fitting procedure of distorted simulations to the experimentally observed diffraction patterns. As an application example, we map the locally varying tetragonality in martensite grains of steel.

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  • Received 17 October 2018
  • Revised 26 November 2018

DOI:https://doi.org/10.1103/PhysRevMaterials.2.123803

©2018 American Physical Society

Physics Subject Headings (PhySH)

Condensed Matter, Materials & Applied Physics

Authors & Affiliations

Aimo Winkelmann1,*, Gert Nolze2,†, Grzegorz Cios3,‡, and Tomasz Tokarski3,§

  • 1Laser Zentrum Hannover e.V., Hollerithallee 8, 30419 Hannover, Germany
  • 2Federal Institute for Materials, Research and Testing (BAM), Unter den Eichen 87, 12205 Berlin, Germany
  • 3Academic Centre for Materials and Nanotechnology, AGH University of Science and Technology, al. A. Mickiewicza 30, 30-059 Krakow, Poland

  • *a.winkelmann@lzh.de
  • gert.nolze@bam.de
  • ciosu@agh.edu.pl
  • §tokarski@agh.edu.pl

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Issue

Vol. 2, Iss. 12 — December 2018

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