Issue 9, 1974
From the journal:

Journal of the Chemical Society, Dalton Transactions

Crystal and molecular structure of trichlorotris(tetrahydrofuran)scandium(III)

J. L. Atwood  and  K. D. Smith  

Abstract

The crystal structure of the title compound has been determined by direct methods from X-ray diffractometer data. Crystals are monoclinic plates, space group P21/c, with Z= 4 in a cell with a= 8·890(4), b= 12·842(6), c= 15·485(6)Å, β= 92·24(5)°. The structure was refined by least-squares techniques to R 0·077 for 1227 unique observed reflections. The substance exists as discrete molecules in which the scandium(III) ion environment is mer-octahedral. Mean Sc–O is 2·18, and mean Sc–Cl 2·41 Å.

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Article information

DOI
https://doi.org/10.1039/DT9740000921
Article type
Paper

J. Chem. Soc., Dalton Trans., 1974, 921-923

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Crystal and molecular structure of trichlorotris(tetrahydrofuran)scandium(III)

J. L. Atwood and K. D. Smith, J. Chem. Soc., Dalton Trans., 1974, 921 DOI: 10.1039/DT9740000921

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