Anchoring of Pd(II) complex in functionalized MCM-41 as an efficient and recoverable novel nano catalyst in C–C, C–O and C–N coupling reactions using Ph3SnCl

Arash Ghorbani-Choghamarani; Farzad Nikpour; Farshid Ghorbani; Forugh Havasi

doi:10.1039/C5RA01934F

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Anchoring of Pd(ii) complex in functionalized MCM-41 as an efficient and recoverable novel nano catalyst in C–C, C–O and C–N coupling reactions using Ph₃SnCl

Arash Ghorbani-Choghamarani,*^a Farzad Nikpour,^b Farshid Ghorbani^c and Forugh Havasi^b

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* Corresponding authors

^a Department of Chemistry, Faculty of Science, Ilam University, P. O. Box 69315516, Ilam, Iran
E-mail: arashghch58@yahoo.com, a.ghorbani@mail.ilam.ac.ir
Fax: +98 841 2227022
Tel: +98 841 2227022

^b Department of Chemistry, Faculty of Sciences, University of Kurdistan, P.O. Box 66315-416, Sanandaj, Iran

^c Department of Environment, Faculty of Natural Resource, University of Kurdistan, Postal code: 66177-15177, Sanandaj, Iran

Abstract

Anchored palladium(II) in functionalized MCM-41 mesoporous silica was prepared and used as an efficient, recoverable and thermally stable heterogeneous nano catalyst for C–C, C–O and C–N bond formation in cross-coupling reactions in the presence of Ph₃SnCl. MCM-41 was prepared trough hydrothermal synthesis using tetraethyl orthosilicate (Si(OC₂H₅)₄) as silica source and cetyltrimethylammonium bromide (CTAB) as a template. The structure of functionalized MCM-41 was studied by FT-IR, XRD, SEM, TEM, TGA, EDS, ICP and BET techniques.

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Article information

DOI: https://doi.org/10.1039/C5RA01934F
Article type: Paper
Submitted: 31 Jan 2015
Accepted: 02 Apr 2015
First published: 02 Apr 2015

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RSC Adv., 2015,5, 33212-33220

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Anchoring of Pd(II) complex in functionalized MCM-41 as an efficient and recoverable novel nano catalyst in C–C, C–O and C–N coupling reactions using Ph₃SnCl

A. Ghorbani-Choghamarani, F. Nikpour, F. Ghorbani and F. Havasi, RSC Adv., 2015, 5, 33212 DOI: 10.1039/C5RA01934F

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