Skip to main content
SpringerLink
Log in

1H and 13C NMR Spectra of 9H-Pyrimido[4,5-b]indoles

  • Published:
Chemistry of Heterocyclic Compounds Aims and scope

Abstract

Based on analysis of 1H and 13C NMR spectra of 9H-pyrimido[4,5-b]indole and its 4-phenyl-2-substituted derivatives, we have made assignments for the signals from the 1H and 13C atoms of these compounds.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

REFERENCES

  1. B. Venugopalan,P. D. Desai, andN. J. de Souza, J. Heterocycl. Chem., 25, 1633 (1988).

    Google Scholar 

  2. C. E. Müller,I. Hide,J. W. Daly,K. Rothenhäusler, andK. Eger, J. Med. Chem., 33, 2822 (1990).

    Google Scholar 

  3. G. L. Bundy,J. R. Palmer, andG. L. Weber, WO Pat. 9626941; Chem. Abstr. 125: 275901 (1996).

    Google Scholar 

  4. G. L. Bundy andJ. R. Palmer, US Pat. 5795986; Chem. Abstr., 129: 175648 (1998).

    Google Scholar 

  5. V. P. Borovik,L. S. Filatova, andV. P. Mamaev, Izv. Siber. Otdel. Akad. Nauk SSSR, Ser. Khim. Nauk, No. 3, 137 (1975).

    Google Scholar 

  6. S. Senda,K. Hirota, andM. Takahashi, J. Chem. Soc., Perkin Trans. 1, 503 (1975).

    Google Scholar 

  7. J. A. Hyatt andJ. S. Swenton, J. Heterocycl. Chem., 9, 409 (1972).

    Google Scholar 

  8. J. A. Hyatt andJ. S. Swenton, J. Org. Chem., 37, 3216 (1972).

    Google Scholar 

  9. T. Higashino,E. Hayashi,H. Matsuda, andT. Katori, Heterocycles, 15, 483 (1981).

    Google Scholar 

  10. J. Bratt,B. Iddon,A. G. Mack,H. Suschitzky,J. A. Taylor, andB. J. Wakefield, J. Chem. Soc., Perkin Trans. 1, 648 (1980).

    Google Scholar 

  11. Y. Kondo,R. Watanabe,T. Sakamoto, andH. Yamanaka, Chem. Pharm. Bull., 37, 2933 (1989).

    Google Scholar 

  12. M. Tielemans,V. Areschka,J. Colomer,R. Promel,W. Langenaeker, andP. Geerlings, Tetrahedron, 48, 10575 (1992).

    Google Scholar 

  13. G. E. Wright, J. Heterocycl. Chem., 13, 539 (1976).

    Google Scholar 

  14. J.-L. Bernier andJ.-P. Henichart, J. Org. Chem., 46, 4197 (1981).

    Google Scholar 

  15. V. V. Lapachev,W. Stadlbauer, andT. Kapper, Monatsh. Chem., 119, 97 (1988).

    Google Scholar 

  16. Yu. N. Portnov,S. N. Bulaga,V. G. Zabrodnyaya, andL. D. Smirnov, Khim. Geterotsikl. Soedin., 400 (1991).

  17. N. PleA. Turck,A. Heynderickx, andG. Queguiner, J. Heterocycl. Chem., 31, 1311 (1994).

    Google Scholar 

  18. K. Eger,W. Lanzner, andK. Rothenhäsler, Liebigs Ann. Chem., 465 (1993).

  19. Sadtler Standard NMR Spectra, Sadtler Research Lab., Philadelphia (1986), 78, 43935.

  20. V. F. Sedova,V. P. Krivopalov, andV. P. Mamaev, Khim. Geterotsikl. Soedin., 986 (1979).

  21. E. Arzel,P. Rocca,F. Marsais,A. Godard, andG. Queguiner, J. Heterocycl. Chem., 34, 1205 (1997).

    Google Scholar 

  22. P. Joseph-Nathan,R. E. del Rio, andM. S. Morales-Rios, Heterocycles, 27, 377 (1988).

    Google Scholar 

  23. J. Riand,M.-T. Chenon, andN. Lumbroso-Bader, Tetrahedron Lett., 3123 (1974).

  24. S. G. Baram,O. P. Shkurko, andV. P. Mamaev, Izv. Akad. Nauk SSSR, Ser. Khim., 686 (1991).

  25. U. Ewers,H. Günter, andL. Jaenicke, Angew. Chem. Int. Ed., 14, 354 (1975).

    Google Scholar 

  26. K. E. Schulte,J. Reisch, andU. Stoess, Arch. Pharm., 305, 523 (1972).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Siberian Branch, Russian Academy of Sciences, Novosibirsk Institute of Organic Chemistry, Novosibirsk, 630090

    V. P. Borovik, M. M. Shakirov, O. P. Shkurko & N. N. Vorozhtsov

Authors
  1. V. P. Borovik
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. M. M. Shakirov
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. O. P. Shkurko
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. N. N. Vorozhtsov
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Borovik, V.P., Shakirov, M.M., Shkurko, O.P. et al. 1H and 13C NMR Spectra of 9H-Pyrimido[4,5-b]indoles. Chemistry of Heterocyclic Compounds 39, 1348–1354 (2003). https://doi.org/10.1023/B:COHC.0000010651.39458.76

Download citation

  • Issue Date:

  • DOI: https://doi.org/10.1023/B:COHC.0000010651.39458.76

Search

Navigation