Elsevier

Additive Manufacturing

Volume 34, August 2020, 101201
Additive Manufacturing

Research Paper
Investigation of the effect of Laser Shock Peening in Additively Manufactured samples through Bragg Edge Neutron Imaging

https://doi.org/10.1016/j.addma.2020.101201Get rights and content

Abstract

Additive manufacturing is a promising and rapidly rising technology in metal processing. However, besides a number of key advantages the constitution of a part through a complex thermo-mechanical process implies also some severe issues with the potential of impacting the quality of products. In laser powder bed fusion (LPBF), the most applied metal additive manufacturing process, the repetitive heating and cooling cycles induce severe strains in the built material, which can have a number of adverse consequences such as deformation, cracking and decreased fatigue life that might lead to severe failure even already during processing. It has been reported recently that the application of laser shock peening (LSP) can counteract efficiently the named issues of LPBF through the introduction of beneficial compressive residual stresses in the surface regions mostly affected by tensile stresses from the manufacturing process. Here we demonstrate how lattice strains implied by LPBF and LSP can efficiently be characterized through diffraction contrast neutron imaging. Despite the spatial resolution need with regards to the significant gradients of the stress distribution and the specific microstructure, which prevent the application of more conventional methods, Bragg edge imaging succeeds to provide essential two-dimensionally spatial resolved strain maps in full field single exposure measurements.

Introduction

Laser powder bed fusion is an additive manufacturing process in which a component is built through layer-wise addition of material [1]. It is a powder bed technique, where a laser selectively melts the powder in a scanning procedure covering the cross section of the component in consecutive layers. After constituting a layer through this procedure, the base is lowered and a new powder layer is deposited and the process repeats. This way the material goes through complex local thermo-mechanical cycles and the solidification of a new layer on an already existing solid layer implies the build-up of detrimental tensile residual stresses due to shrinkage during cooling of the top layers [2,3]. Despite competitive material properties achieved nowadays in many cases through process optimization [[4], [5], [6], [7], [8], [9], [10]], these complex stress states can cause distortions, cracking and even delamination and complete process failures during the build process [2,3,11].

A variety of in-situ and post-processing techniques have been developed and applied to circumvent the issues. Post-processing cannot prevent process failure and most techniques have severe limitations and drawbacks. For example, pre-heating and laser re-melting can reduce tensile residual stresses and improve geometrical accuracy, but they are limited in introducing compressive stresses and improving fatigue life, hardness, microstructure and crack density [12]. Similar is true for post process heat and hot isostatic pressing (HIP) treatments, which, while improving density through crack closure, can even negatively affect the microstructure and hence properties such as yield strength through promoting significant grain growth [[13], [14], [15]].

Recently, a novel and very promising approach has been introduced. Laser shock peening (LSP) has previously been applied successfully to conventionally produced components to introduce beneficial compressive residual stresses in the surface region and thus increase fatigue life. LSP is a well-known surface treatment. It is used for the purpose of introducing plastic deformation and compressive residual stresses (CRS) into the subsurface region of the treated material. A high energy laser with a pulse duration in the nanosecond range is directed at the surface of the sample. The high energy laser pulse ablates a shallow layer of the surface thus creating a high pressure shockwave directed towards the bulk of the sample. This shockwave plastically deforms the material thus introducing CRS in the subsurface region [16]. Now it could be shown, that LSP applied to LPBF parts has the ability to convert the tensile residual stresses produced by LPBF into beneficial compressive stresses in the processed surface region [17]. In addition to that, it could be proven that LSP can be applied in a hybrid LPBF process referred to as 3D-LSP [18], which allows to apply LSP at any chosen layer of the build process, where it does not only enable stress fields but local microstructure to be tailored to specific requirements [19,20]. The implied compressive stresses also support crack healing, geometrical integrity and increase in fatigue life [21,22]

Section snippets

Method

Here we introduce an advanced approach for the inspection and investigation of additively manufactured and particularly LSP treated samples. While conventional non-destructive investigation techniques [23] reach their limits due to grain sizes, strain gradients, hence required spatial resolution, and material depths to be assessed, Bragg edge neutron imaging [24] appears well suited to visualize strain fields with the required resolution [25]. Bragg edge imaging is capable to map lattice

Samples

In order to investigate the potential of Bragg edge imaging to resolve the strains and thus the strain gradient in the surface region of LPBF and LSP treated LPBF samples with sufficient spatial and strain resolution two additively manufactured samples were chosen for a proof-of-principle experiment. Both samples are cuboids of 316 L austenitic stainless steel build by LPBF. The powder was DIAMALLOY 1003, obtained from Oerlikon Metco, Switzerland. The chemical composition is shown in Table 1.

Results and discussion

The application of pixel-wise fitting of the Bragg edge in the attenuation spectrum enables a mapping of the local (111) lattice parameter d111 with high resolution (Fig. 3). It clearly displays the expected features of a relatively homogeneous heat treated reference sample, and larger lattice spacings in particular at the edges of the as built (non heat treated) sample where tensile stresses are to be expected. At the lower left edge of the as built sample, where the LSP treatment has been

Conclusions

It has been demonstrated, that high resolution Bragg edge imaging can provide full field maps of strain distributions in additively manufactured samples. The method is capable of visualizing the inhomogeneous strain distribution from the surface to the bulk of the material, from tensile to compressive strains. In particular an application to a sample partially treated by laser shock peening on one surface demonstrates the potential of the non-destructive spatially resolved mapping of strains

CRediT authorship contribution statement

M. Morgano: Software, Validation, Formal analysis, Investigation, Data curation, Writing - original draft, Writing - review & editing, Visualization. N. Kalentics: Validation, Investigation, Resources, Writing - review & editing. C. Carminati: Software, Validation, Writing - review & editing. J. Capek: Visualization, Writing - review & editing, Funding acquisition. M. Makowska: Investigation, Resources, Writing - review & editing. R. Woracek: Investigation, Writing - review & editing. T.

Declaration of Competing Interest

The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Acknowledgements

The work was partially funded through the OP RDE, MEYS, under the project “European Spallation Source–participation of the Czech Republic—OP”, Reg. No. CZ.02.1.01/0.0/0.0/16 013/0001794, MS, JC, RL, TM additionally thank for financial support from the Strategic Focus Area Advanced Manufacturing (SFA-AM), an initiative of the ETH Board, and JC also for funding from the European Union’s Horizon 2020 research and innovation programme under the Marie Skłodowska-Curie grant agreement No 701647. The

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