Abstract
Commercial pure copper sheets were severely deformed after primary annealing to a strain magnitude of 2.32 through constrained groove pressing. After induction of an electrical current, the sheets were heated for 0.5, 1, 2, or 3 s up to maximum temperatures of 150, 200, 250, or 300°C. To compare the annealing process in the current-carrying system with that in the current-free system, four other samples were heated to 300°C at holding times of 60, 90, 120, or 150 s in a salt bath. The microstructural evolution and hardness values of the samples were then investigated. The results generally indicated that induction of an electrical current could accelerate the recrystallization process by decreasing the thermodynamic barriers for nucleation. In other words, the current effect, in addition to the thermal effect, enhanced the diffusion rate and dislocation climb velocity. During the primary stages of recrystallization, the grown nuclei of electrically annealed samples showed greater numbers and a more homogeneous distribution than those of the samples annealed in the salt bath. In the fully recrystallized condition, the grain size of electrically annealed samples was smaller than that of conventionally annealed samples. The hardness values and metallographic images obtained indicate that, unlike the conventional annealing process, which promotes restoration phenomena with increasing heating time, the electrical annealing process does not necessarily promote these phenomena. This difference is hypothesized to stem from conflicts between thermal and athermal effects during recrystallization.
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The authors wish to thank the research board of Sharif University of Technology for the financial support and the provision of the research facilities used in this work.
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Nobakht, S., Kazeminezhad, M. Electrical annealing of severely deformed copper: microstructure and hardness. Int J Miner Metall Mater 24, 1158–1168 (2017). https://doi.org/10.1007/s12613-017-1506-2
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DOI: https://doi.org/10.1007/s12613-017-1506-2