Abstract
The effect of microwave radiation on the nucleation and crystallization of tailing-based glass-ceramics was investigated using a 2.45 GHz multimode microwave cavity. Tailing-based glass samples were prepared from Shandong gold tailings and Guyang iron tailings utilizing a conventional glass melting technique. For comparison, the tailing-based glass samples were crystallized using two different heat-treatment methods: conventional heating and hybrid microwave heating. The nucleation and crystallization temperatures were determined by performing a differential thermal analysis of the quenched tailing-based glass. The prepared glass-ceramic samples were further characterized by Fourier transform infrared spectroscopy, X-ray diffraction, Raman spectroscopy, thermal expansion coefficient measurements, and scanning electron microscopy. The results demonstrated that hybrid microwave heating could be successfully used to crystallize the tailing-based glass, reduce the processing time, and decrease the crystallization temperature. Furthermore, the results indicated that the nucleation and crystallization mechanism of the hybrid microwave heating process slightly differs from that of the conventional heating process.
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H.J. Wang, Q.X. Liu, and P. Xu, Economic analysis and cases of large-scale utilization of tailings, Met. Mine, 2014, No. 9, p. 147.
M. Erol, A. Genç, M.L. Öveçoglu, E. Yücelen, S. Küçükbayrak, and Y. Taptik, Characterization of a glass-ceramic produced from thermal power plant fly ashes, J. Eur. Ceram. Soc., 20(2000), No. 12, p. 2209.
Y.J. Park and J. Heo, Conversion to glass-ceramics from glasses made by MSW incinerator fly ash for recycling, Ceram. Int., 28(2002), No. 6, p. 689.
R.D. Rawlings, J.P. Wu, and A.R. Boccaccini, Glass-ceramics: Their production from wastes: a review, J. Mater. Sci., 41(2006), No. 3, p. 733.
M.L. Öveçoglu, Microstructural characterization and physical properties of a slag-based glass-ceramic crystallized at 950 and 1100°C, J. Eur. Ceram. Soc., 18(1998), No. 2, p. 161.
B.W. Li, Y.S. Du, X.F. Zhang, X.L. Jia, M. Zhao, and H. Chen, Effects of iron oxide on the crystallization kinetics of Baiyunebo tailing glass-ceramics, Tran. Indian Ceram. Soc., 72(2013), No. 2, p. 119.
B.W. Li, L.B. Deng, X.F. Zhang, and X.L. Jia, Structure and performance of glass-ceramics obtained by Bayan Obo tailing and fly ash, J. Non Cryst. Solids, 380(2013), p. 103.
A.A. Francis, Conversion of blast furnace slag into new glass-ceramic material, J. Eur. Ceram. Soc., 24(2004), No. 9, p. 2819.
Y. Tian, W. Zuo, and D.D. Chen, Crystallization evolution, microstructure and properties of sewage sludge-based glass-ceramics prepared by microwave heating, J. Hazard. Mater., 196(2011), p. 370.
S. Das, A.K. Mukhopadhyay, S. Datta, G.C. Das, and D. Basu, Hard glass-ceramic coating by microwave processing, J. Eur. Ceram. Soc., 28(2008), No. 4, p. 729.
C. Siligardi, C. Leonelli, F. Bondioli, A. Corradi, and G.C. Pellacani, Densification of glass powders belonging to the CaO–ZrO2–SiO2 system by microwave heating, J. Eur. Ceram. Soc., 20(2000), No. 2, p. 177.
F.J.M. Almeida, J.R. Martinelli, and C.S.M. Partiti, Characterization of iron phosphate glasses prepared by microwave heating, J. Non Cryst. Solids, 353(2007), No. 52-54, p. 4783.
M.M. Mahmoud, D.C. Folz, C.T.A. Suchicital, and D.E. Clark, Crystallization of lithium disilicate glass using microwave processing, J. Am. Ceram. Soc., 95(2012), No. 2, p. 579.
J.S. Chen, H. Li, L.Y. Tang, and F. He, Glass-ceramics, Chemical Industry Press, Beijing, 2006, p. 75.
B.W. Li, Y.S. Du, X.F. Zhang, M. Zhao, and H. Chen, Crystallization characteristics and properties of high-performance glass-ceramics derived from Baiyunebo east mine tailing, Environ. Prog. Sustainable Energy, 34(2014), No. 2, p. 420.
R.D. Shannon, Revised effective ionic radii and systematic studies of interatomic distances in halides and chalcogenides, Acta Cryst., A32(1976), p. 751.
J. Jacob, L.H.L. Chia, and F.Y.C. Boey, Thermal and non-thermal interaction of microwave radiation with materials, J. Mater. Sci., 30(1995), No. 21, p. 5321.
M. Okuno, N. Zotov, M. Schmücker, and H. Schneider, Structure of SiO2-Al2O3 glasses: combined X-ray diffraction, IR and Raman studies, J. Non Cryst. Solids, 351 (2005), No. 12-13, p. 1032.
S. Atalay, H.I. Adiguzel, and F. Atalay, Infrared absorption study of Fe2O3-CaO-SiO2 glass ceramics, Mater. Sci. Eng. A, 304-306(2001), p. 796.
S. Shoval, E. Yadin, and G. Panczer, Analysis of thermal phases in calcareous Iron Age pottery using FT-IR and Raman spectroscopy, J. Therm. Anal. Calorim., 104(2011), No. 2, p. 515.
S.Y. Yao, Z.F. Wang, Y. Han, and W.W. Zhang, Preparation and structure analysis of diopside glass-ceramics from coal fly-ash, Trans. Mater. Heat Treat., 34(2013), No. 7, p. 22.
D.U. Tulyaganov, S. Agathopoulos, J.M. Ventura, M.A. Karakassides, O. Fabrichnaya, and J.M.F. Ferreira, Synthesis of glass-ceramics in the CaO-MgO-SiO2 system with B2O3, P2O5, Na2O and CaF2 additives, J. Eur. Ceram. Soc., 26(2006), No. 8, p. 1463.
P. McMillan, A Raman spectroscopic study of glasses in the system CaO-MgO-SiO2, Am. Mineral., 69(1984), p. 645.
B.W. Li, S.L. Ouyang, X.F. Zhang, X.L. Jia, L.B. Deng, and F. Liu, Effect of temperature on the structure of CaO-MgO-Al2O3-SiO2 nanocrystalline glass-ceramics studied by Raman spectroscopy, Spectrosc. Spect. Anal., 34(2014), No. 7, p. 1869.
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Li, Bw., Li, Hx., Zhang, Xf. et al. Nucleation and crystallization of tailing-based glass-ceramics by microwave heating. Int J Miner Metall Mater 22, 1342–1349 (2015). https://doi.org/10.1007/s12613-015-1203-y
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DOI: https://doi.org/10.1007/s12613-015-1203-y