Skip to main content
Log in

Investigation on the dissolution of η phase in a cast Ni-based superalloy

  • Published:
International Journal of Minerals, Metallurgy, and Materials Aims and scope Submit manuscript

Abstract

The dissolution behavior of η phase has been investigated in a cast Ni-based superalloy. The results showed that the platelets and blocks of η phase were formed within the interdendritic regions of the microstructure. Applying standard solution annealing at 1150–1160°C for a period of 4 h did not result in the complete dissolution of η phase. For the complete dissolution of η phase without residual incipient melting, a 2-step solution annealing has been recommended. After dissolution at high temperatures, the η phase transforms to two MC-type carbides: one is enriched in Ti, Nb, and Ta, and the other is of (Zr,Ti)C type.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. T. B. Gibbons and R. Stickler, IN939: metallurgy, properties and performances, [in] Proceeding of High Temperature Alloys for Gas Turbines, Liège, 1982, p. 369.

  2. K. M. Delargy and G.D.W. Smith, Phase composition and phase stability of a high-chromium nickel-based superalloy, IN939, Metall. Trans. A, 14(1983), No. 9, p. 1771.

    Article  Google Scholar 

  3. M. T. Jovanovića, Z. Miškovića, and B. Lukića, Microstructure and stress-rupture life of polycrystal, directionally solidified and single crystal casting on nickel based IN 939 superalloy, Mater. Charact., 40(1998), No. 4–5, p. 261.

    Article  Google Scholar 

  4. K. M. Delargy, S.W.K. Shaw, and G.D.W. Smith, Effects of heat treatment on mechanical properties of high-chromium nickel-base superalloy IN 939, Mater. Sci. Technol., 2(1986), No. 10, p. 1031.

    Article  CAS  Google Scholar 

  5. R. W. Hatala and J.J. Schirra, Development of a damage tolerant heat treatment for cast + HIP Incoloy 939, [in] Superalloys 1996, TMS, Warrendale, 1996, p. 137.

  6. S. W.K. Shaw, Response of IN-939 to process variations, [in] Superalloys 1980, Champion, 1980, p. 275.

  7. G. K. Bouse, Eta and platelet phases in investment cast superalloys, [in] Superalloys 1996, TMS, Warrendale, 1996, p. 163.

    Google Scholar 

  8. L. Wang, Y.J. Yao, B. Liu, B.Y. Zhong, and J.X. Dong, Effect of cooling rate on the phase transformation and stability of the mushy zone during the solidification of Waspaloy, Int. J. Miner. Metall. Mater., 17(2010), No. 4, p. 464.

    Article  CAS  Google Scholar 

  9. L. Xu, C.Y. Cui, and X.F. Sun, The effects of Co and Ti additions on microstructures and compressive strength of Udimet710, Mater. Sci. Eng. A, 528(2011), No. 27, p. 7851.

    Article  CAS  Google Scholar 

  10. C. Y. Cui, Y.F. Gu, D.H. Ping, and H. Harada, Microstructural evolution and mechanical properties of a Ni-based superalloy, TMW-4, Metall. Mater. Trans. A, 40(2009), No. 2, p. 282.

    Article  Google Scholar 

  11. S. T. Wlodek, M. Kelly, and D.A. Alden, The structure of Rene 88DT, [in] Superalloys 1996, TMS, Warrendale, 1996, p. 129.

    Google Scholar 

  12. J. B. Wahl and K. Harris, Advanced Ni base superalloys for small gas turbines, Can. Metall. Q., 50(2011), No. 3, p. 207.

    Article  CAS  Google Scholar 

  13. F. Long, Y.S. Yoo, C.Y. Jo, S.M. Seo, Y.S. Song, T. Jin, and Z.Q. Hu, Formation of η and σ phase in three polycrystalline superalloys and their impact on tensile properties, Mater. Sci. Eng. A, 527(2009), No. 1–2, p. 361.

    Google Scholar 

  14. E. F. Bradley, Superalloys: A Technical Guide, ASM International, Metals Park, Ohio, 1988, p. 32.

    Google Scholar 

  15. J. R. Davis, Heat Resistant Materials, ASM Specialty Handbook, ASM International, Materials Park, Ohio, 1997, p. 226.

    Google Scholar 

  16. X. Z. Qin, J.T. Guo, C. Yuan, J.S. Hou, and H.Q. Ye, Degeneration of primary MC carbide in a cast Ni-base superalloy, Mater. Sci. Forum, 546–549(2007), p. 1301.

    Article  Google Scholar 

  17. B. G. Choi, I.S. Kim, D.H. Kim, and C.Y. Jo, Temperature dependence of MC decomposition behavior in Ni-base superalloy GTD 111, Mater. Sci. Eng. A, 478(2008), No. 1–2, p. 329.

    Google Scholar 

  18. X. Z. Qin, J.T. Guo, C. Yuan, J.S. Hou, and H.Q. Ye, Thermal stability of primary carbides and carbonitrides in two cast Ni-base superalloys, Mater. Lett., 62(2008), No. 15, p. 2275.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to M. R. Jahangiri.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Jahangiri, M.R., Arabi, H. & Boutorabi, S.M.A. Investigation on the dissolution of η phase in a cast Ni-based superalloy. Int J Miner Metall Mater 20, 42–48 (2013). https://doi.org/10.1007/s12613-013-0691-x

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s12613-013-0691-x

Keywords

Navigation