Skip to main content

Advertisement

Log in

Effect of Al Addition on the Rolled Microstructure and Mechanical Properties of Mg-4Y-3Nd Alloys

  • Technical Article
  • Published:
Journal of Materials Engineering and Performance Aims and scope Submit manuscript

Abstract

The effect of Al contents (0, 0.5, 1.0 and 1.5 wt.%) on the microstructure evolution, texture and mechanical properties of Mg-4Y-3Nd alloys rolled sheets were investigated. The results showed that the Al2RE phase was formed when Al was added into the as-cast alloys, which could refine the microstructure of the alloys. After homogenization treatment, the Al2RE phase was insoluble, and the Al2RE phase at the grain boundaries could pin the grain boundaries to prevent grain growth. The Al-containing alloys had good grain thermal stability. The Al2RE phase promoted dynamic recrystallization (DRX) through the particle-stimulated nucleation (PSN) mechanism and refined recrystallized grains during the rolling process. Al refinement will affect the texture type and strength of the alloy. The addition of 0.5 wt.% Al could improve the texture intensity, and a further increase in Al would reduce the texture intensity. When the Al content was 1.5 wt.%, the alloy had the smallest recrystallized grains, the weakest texture intensity, and the best mechanical properties. The tensile strength, yield strength and elongation were 264.4, 225.3 MPa and 9.4%, respectively.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14

Similar content being viewed by others

References

  1. Y.H. Chen, L.P. Wang, Y.C. Feng, L. Wang, and E.J. Guo, Effect of Al Content on Hot Tearing Behaviour of Mg-xAl-2Ca-2Sm Alloys, Mater. Sci. Technol., 2019, 35, p 116–126.

    Article  Google Scholar 

  2. J.X. Zhou, Y.S. Yang, W.H. Tong, J.W.J.W. Fu, and B. Wang, Effect of Cooling Rate on the Solidified Microstructure of Mg-Gd-Y-Zr Alloy, Rare. Metal. Mater. Eng., 2010, 39, p 1899–1902.

    Article  Google Scholar 

  3. J.H. Zhang, S.J. Liu, R.Z. Wu, L.G. Hou, and M.L. Zhang, Recent Developments in High-Strength Mg-RE-Based Alloys: Focusing on Mg-Gd and Mg-Y Systems, J. Magnes. Alloys, 2018, 6, p 277–291.

    Article  Google Scholar 

  4. Z.L. Ning, J.Y. Yi, M. Qian, H.C. Sun, F.Y. Cao, H.H. Liu, and J.F. Sun, Microstructure and Elevated Temperature Mechanical and Creep Properties of Mg-4Y-3Nd-0.5Zr Alloy in the Product Form of a Large Structural Casting, Mater. Des., 2014, 60, p 218–225.

    Article  Google Scholar 

  5. Y.H. Ali, D. Qiu, B. Jiang, F.S. Pan, and M.X. Zhang, Current Research Progress in Grain Refinement of Cast Magnesium Alloys: A Review Article, J. Alloys. Compd., 2015, 619, p 639–651.

    Article  Google Scholar 

  6. D.H. Stjohn, M.A. Easton, M. Qian, and J.A. Taylor, Grain Refinement of Magnesium Alloys: A Review of Recent Research, Theoretical Developments, and Their Application, Metall. Mater. Trans. A, 2013, 44A, p 2935–2949.

    Article  Google Scholar 

  7. J.Y. Yi, Z.L. Ning, and J.F. Sun, Effect of Grain Size on the Microstructure and Mechanical Properties of Mg-4Y-3Nd-0.5Zr Alloy, Int. J. Mater. Res., 2014, 105, p 607–609.

    Article  Google Scholar 

  8. D. Qiu, M.A. Zhang, J.X. Taylor, and P.M. Kelly, A New Approach to Designing a Grain Refiner for Mg Casting Alloys and its Use in Mg-Y-Based Alloys, Acta Mater., 2009, 57, p 3052–3059.

    Article  Google Scholar 

  9. J.C. Dai, S.M. Zhu, M.A. Easton, M.X. Zhang, D. Qiu, and G.H. Wu, Heat treatment, Microstructure and Mechanical Properties of a Mg-Gd-Y Alloy Grain-Refined by Al Additions, Mater. Sci. Eng. A, 2013, 576, p 298–305.

    Article  Google Scholar 

  10. X.B. Zheng, W.B. Du, Z.H. Wang, S.B. Li, K. Liu, and X. Du, Remarkably Enhanced Mechanical Properties of Mg-8Gd-1Er-0.5Zr Alloy on the Route of Extrusion, Rolling and Aging, Mater. Lett., 2018, 212, p 155–158.

    Article  Google Scholar 

  11. R. Zhu, C.J. Bian, and Y.J. Wu, Mechanical Properties and Microstructural Evolution of Variable-Plane-Rolled Mg-3Al-1Zn Alloy, J. Mater. Eng. Perform., 2017, 26, p 2937–2946.

    Article  Google Scholar 

  12. P. Emadi and C. Ravindran, The Influence of High Temperature Ultrasonic Processing Time on the Microstructure and Mechanical Properties AZ91E Magnesium Alloy, J. Mater. Eng. Perform., 2021, 30, p 1188–1199.

    Article  Google Scholar 

  13. Y.J. Wu and R. Zhu, Effect of Rolling Temperature on the Microstructure and Mechanical Properties of AZ31 Alloy Sheet Processed through Variable-Plane Rolling, J. Mater. Eng. Perform., 2019, 28, p 6182–6191.

    Article  Google Scholar 

  14. L. Zheng, C.M. Liu, J. Jin, X. Wang, and D.W. Ji, Effect of Hot-Rolling on Microstructures and Mechanical Properties of Extruded Mg-6Gd-3.2Y-xZn-0.5Zr Sheet, J. Mater. Eng. Perform., 2013, 22, p 104–111.

    Article  Google Scholar 

  15. B. Li, J. Wu, and B.G. Teng, Influences of the Texture Characteristic and Interdendritic LPSO Phase Distribution on the Tensile Properties of Mg-Gd-Y-Zn-Zr Sheets Through Hot Rolling, Acta Metall. Sin., 2021, 34, p 1051–1064.

    Article  Google Scholar 

  16. J.B. Shao, Z.Y. Chen, T. Chen, and C.M. Liu, Deformation Mechanism of Mg-Gd-Y-Zn-Zr Alloy Containing Long-Period Stacking Ordered Phases During Hot Rolling, Metall. Mater. Trans. A, 2020, 51, p 1911–1923.

    Article  Google Scholar 

  17. J.B. Shao, Z.Y. Chen, T. Chen, and C.M. Liu, The Interaction Between 10(1)over-bar2 Twinning and Long-Period Stacking Ordered (LPSO) Phase During Hot Rolling and Annealing Process of a Mg-Gd-Y-Zn-Zr Alloy, Metall. Mater. Trans. A, 2021, 52, p 520–530.

    Article  Google Scholar 

  18. C.F. Fang, G.X. Liu, X.T. Liu, H. Hao, and X.G. Zhang, Significant Texture Weakening of Mg-8Gd-5Y-2Zn Alloy by Al Addition, Mater. Sci. Eng. A, 2017, 701, p 314–318.

    Article  Google Scholar 

  19. C.F. Fang, G.X. Liu, H. Hao, Z.H. Wen, and X.G. Zhang, Effect of Al Addition on Microstructure, Texture and Mechanical Properties of Mg-5Gd-2.5Y-2Zn Alloy, J. Alloys. Compd., 2016, 686, p 347–355.

    Article  Google Scholar 

  20. L. Wang, E.J. Guo, W.Y. Jiang, Y.C. Feng, S.C. Zhao, F.K. Fu, and H.T. Chen, Effect of Al Addition on Microstructure and Mechanical Properties of As-Cast Mg-4Y-3Nd Alloy, Philos. Mag., 2020, 100, p 234–247.

    Article  Google Scholar 

  21. Y.P. Zhuang, P.W. Zhou, H.X. Wang, K.B. Nie, Y.M. Liu, W. Liang, L.F. Wang, and L.W. Zheng, The Formation Mechanism of the Lamellar Phase Precipitated During Solid Solution Treatment in the Mg-Gd-Al Alloy, J. Mater. Res. Technol., 2020, 9, p 11392–11401.

    Article  Google Scholar 

  22. Y.C. Feng, L. Wang, Y. Fu, S.C. Zhao, and E.J. Guo, Effect of Heat Treatment on Microstructure and Mechanical Properties of Mg-4Y-3Nd-1.5Al Alloy, Rare. Metal. Mater. Eng., 2021, 50, p 1826–1832.

    Google Scholar 

  23. Z.B. Chen, C.M. Liu, H.C. Xiao, J.K. Wang, Z.Y. Chen, S.N. Jiang, and Z.J. Su, Effect of Rolling Passes on the Microstructures and Mechanical Properties of Mg-Gd-Y-Zr Alloy Sheets, Mater. Sci. Eng. A, 2014, 618, p 232–237.

    Article  Google Scholar 

  24. X.L. Hou, Z.Y. Cao, L. Zhao, L.D. Wang, Y.M. Wu, and L.M. Wang, Microstructure, Texture and Mechanical Properties of a Hot Rolled Mg-6.5Gd-1.3Nd-0.7Y-0.3Zn Alloy, Mater. Des., 2012, 34, p 776–781.

    Article  Google Scholar 

  25. J.D. Robson, D.T. Henry, and B. Davis, Particle Effects on Recrystallization in Magnesium-Manganese Alloys: Particle-Stimulated Nucleation, Acta Mater., 2009, 57, p 2739–2747.

    Article  Google Scholar 

  26. G.H. Huang, D.D. Yin, J.W. Lu, H. Zhou, Y. Zeng, G.F. Quan, and Q.D. Wang, Microstructure, Texture and Mechanical Properties Evolution of Extruded Fine-Grained Mg-Y Sheets During Annealing, Mater. Sci. Eng. A, 2018, 720, p 24–35.

    Article  Google Scholar 

  27. S.G. Kim and Y.B. Park, Grain Boundary Segregation, Solute Drag and Abnormal Grain Growth, Acta Mater., 2008, 56, p 3739–3753.

    Article  Google Scholar 

  28. S.G. Hong, S.H. Park, and C.S. Lee, Role of 10–12 Twinning Characteristics in the Deformation Behavior of a Polycrystalline Magnesium Alloy, Acta Mater., 2010, 58, p 5873–5885.

    Article  Google Scholar 

  29. J.D. Robson, S.J. Haigh, B. Davis, and D. Griffiths, Grain Boundary Segregation of Rare-Earth Elements in Magnesium Alloys, Metall. Mater. Trans. A, 2016, 47, p 522–530.

    Article  Google Scholar 

  30. S.H. Park, H. Yu, J.H. Bae, C.D. Yim, and B.S. You, Microstructural Evolution of Indirect-Extruded ZK60 Alloy by Adding Ce, J. Alloys. Compd., 2012, 545, p 139–143.

    Article  Google Scholar 

  31. Q. Wen, K.K. Deng, J.Y. Shi, B.P. Zhang, and W. Liang, Effect of Ca Addition on the Microstructure and Tensile Properties of Mg-4.0Zn-2.0Gd Alloys, Mater. Sci. Eng. A, 2014, 609, p 1–6.

    Article  Google Scholar 

  32. H.H. Yu, Y.C. Xin, M.Y. Wang, and Q. Liu, Hall-Petch Relationship in Mg Alloys: A Review, Mater. Sci. Technol., 2018, 34, p 248–256.

    Article  Google Scholar 

  33. B. Li, B.G. Teng, and E.D. Wang, Effects of Accumulative Rolling Reduction on the Microstructure Characteristic and Mechanical Properties of Mg-Gd-Y-Zn-Zr Sheets Processed by Hot Rolling, Mater. Sci. Eng. A, 2019, 765, 138317.

    Article  Google Scholar 

  34. Q.H. Wang, B. Jiang, A.T. Tang, C. He, D.F. Zhang, J.F. Song, T.H. Yang, G.S. Huang, and F.S. Pan, Formation of the Elliptical Texture and its Effect on the Mechanical Properties and Stretch Formability of Dilute Mg-Sn-Y Sheet by Zn Addition, Mat. Sci. Eng. A-Struct., 2019, 746, p 259–275.

    Article  Google Scholar 

  35. S. Najafi, Y. Palizdar, A. Sheikhani, and M.F.S.M.H. Soltan Ali NezhadAbdiyanBanijamaliTorkamani, The Effect of Y Addition on the Microstructure and Work Hardening Behavior of Mg-Zn-Zr Alloys, J. Mater. Eng. Perform., 2021, 30, p 2574–2585.

    Article  Google Scholar 

  36. Z.B. Chen, C.M. Liu, H.C. Xiao, and J.K.Z.Y.S.N.Z.J. WangChenJiangSu, Effect of Rolling Passes on the Microstructures and Mechanical Properties of Mg-Gd-Y-Zr Alloy Sheets, Mat. Sci. Eng. A-Struct., 2014, 618, p 232–237.

    Article  Google Scholar 

Download references

Acknowledgment

The authors gratefully acknowledge the financial support from the Major Special Project of Heilongjiang Province (No.2020ZX03A03); The authors gratefully acknowledge the financial support from the Heilongjiang Province Natural Science Foundation (E2018045).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Lei Wang.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Cao, Y., Wang, L., Guo, E. et al. Effect of Al Addition on the Rolled Microstructure and Mechanical Properties of Mg-4Y-3Nd Alloys. J. of Materi Eng and Perform 31, 8699–8710 (2022). https://doi.org/10.1007/s11665-022-06980-5

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11665-022-06980-5

Keywords

Navigation