The effect of deep cryogenic treatment (DCT) on microstructure and mechanical properties including corrosion behavior of the squeeze-cast AE42 alloy has been investigated. For comparison, the same has also been studied on the untreated alloy. Both the untreated and deep cryogenic-treated (DCTed) alloys comprised α-Mg and Al4RE phases. Volume fraction of the Al4RE phase in the AE42 alloy reduced gradually following DCT carried out from 4 to 16 h. Ductility and UTS increase significantly with a marginal increase in YS of all the DCTed alloys. The improvement was attributed to the dissolution of the brittle Al4RE phase following DCT. Among the alloys employed, the best tensile properties were obtained for the 16-h DCT alloy due to its lowest content of the brittle Al4RE phase. Creep resistance of the DCTed alloys was lower than that of the untreated alloy owing to the presence of less amount of thermally stable intermetallic Al4RE phase. Wear resistance of the alloy reduces following DCT due to reduced hardness of the DCTed alloys. The untreated alloy exhibits the best corrosion resistance, whereas poor corrosion resistance of the DCTed alloys is attributed to the reduced amount of Al4RE phase that fails to built a corrosion resistance barrier.
Similar content being viewed by others
References
B.L. Mordike and T. Ebert, Magnesium: Properties-Applications-Potential, Mater. Sci. Eng. A, 2001, 302, p 37
K.M. Asl, A. Tari, and F. Khomamizadeh, Effect of Deep Cryogenic Treatment on Microstructure, Creep and Wear Behaviors of AZ91 Magnesium Alloy, Mater. Sci. Eng. A, 2009, 523, p 27
P. Baldissera and C. Delprete, Deep cryogenic Treatment: A Bibliographic Review, Open Mech. Eng. J., 2008, 2, p 1
A. Bensely, A. Prabhakaran, D. Mohan Lal, and G. Nagarajan, Enhancing the Wear Resistance of Case Carburized Steel (En 353) by Cryogenic Treatment, Cryogenics (Guildf), 2005, 45, p 747
H.H. Liu, J. Wang, B.L. Shen, H.S. Yang, S.J. Gao, and S.J. Huang, Effects of Deep Cryogenic Treatment on Property of 3Cr13Mo1V1.5 High Chromium Cast Iron, Mater. Des., 2007, 28, p 1059
S. Zhirafar, A. Rezaeian, and M. Pugh, Effect of Cryogenic Treatment on the Mechanical Properties of 4340 Steel, J. Mater. Process. Technol., 2007, 186, p 298
V. Firouzdor, E. Nejati, and F. Khomamizadeh, Effect of Deep Cryogenic Treatment on Wear Resistance and Tool Life of M2 HSS Drill, J. Mater. Process. Technol., 2008, 206, p 467
Y.M. Rhyim, S.H. Han, Y.S. Na, and J.H. Lee, Effect of Deep Cryogenic Treatment on Carbide Precipitation and Mechanical Properties of Tool Steel, Solid State Phenom., 2006, 118, p 9
K. Amini, A. Akhbarizadeh, and S. Javadpour, Investigating the Effect of Quench Environment and Deep Cryogenic Treatment on the Wear Behavior of AZ91, Mater. Des., 2014, 54, p 154
Y. Jiang, D. Chen, Z. Chen, and J. Liu, Effect of Cryogenic Treatment on the Microstructure and Mechanical Properties of AZ31 Magnesium Alloy, Mater. Manuf. Process., 2010, 25, p 837
G.L. Song and A. Atrens, Corrosion Mechanisms of Magnesium Alloys, Adv. Eng. Mater., 1999, 1, p 11
B.R. Powell, V. Rezhets, M.P. Balogh, and R.A. Waldo, Microstructure and Creep Behavior in AE42 Magnesium Die-Casting Alloy, JOM, 2002, 54, p 34
A.K. Mondal and S. Kumar, Impression Creep Behaviour of Magnesium Alloy-Based Hybrid Composites in the Transverse Direction, Compos. Sci. Technol., 2009, 69, p 1592
A.K. Mondal, C. Blawert, and S. Kumar, Corrosion Behaviour of Creep-Resistant AE42 Magnesium Alloy-Based Hybrid Composites Developed for Powertrain Applications, Mater. Corros., 2015, 66, p 1150–1158
J. Liu, G. Li, D. Chen, and Z. Chen, Effect of Cryogenic Treatment on Deformation Behavior of As-Cast AZ91 Mg Alloy, Chin J. Aeronaut., 2012, 25, p 931
ASM Specialty Handbook: Magnesium and Magnesium Alloys, Ed. M. Avedesian, H. Baker.
Z.R. Liu and D.Y. Li, The Electronic Origin of Strengthening and Ductilizing Magnesium by Solid Solutes, Acta Mater., 2015, 89, p 225
M. Suzuki, H. Sato, K. Maruyama, and H. Oikawa, Creep Behavior and Deformation Microstructures of Mg–Y Alloys at 550 K, Mater. Sci. Eng. A, 1998, 252, p 248
L. Gao, R.S. Chen, and E.H. Han, Effects of Rare-Earth Elements Gd and Y on the Solid Solution Strengthening of Mg Alloys, J. Alloys Compd., 2009, 481, p 379
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Bhale, P., Shastri, H., Mondal, A.K. et al. Effect of Deep Cryogenic Treatment on Microstructure and Properties of AE42 Mg Alloy. J. of Materi Eng and Perform 25, 3590–3598 (2016). https://doi.org/10.1007/s11665-016-2238-6
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11665-016-2238-6