Abstract
In order to solve the problems of coal spontaneous combustion, poor inerting effect of traditional nitrogen injection, and waste of resources in goaf, based on the response surface methodology and Box-Behnken combination test principle, the self-developed continuous and precise nitrogen injection and fire-fighting equipment was used to study the best possible combination of nitrogen injection position (20–90 m), nitrogen injection amount (10–70 m3/min), and air supply volume (2100–2500 m3/min), aiming to minimize the width of the oxidation zone and CO concentration in goaf. The optimal key parameters of continuous precise nitrogen injection were determined as follows: nitrogen injection position 54.17 m, nitrogen injection amount 31.04 m3/min, and air supply 2484.81 m3/min. Under this condition, the width of the oxidation zone was 29.21 ± 0.3 m and the CO concentration was 28.1 ± 4.4 ppm, which were similar to the predicted results of the model (the width of the oxidation zone was 29.41 m; CO concentration was 27.28 ppm). The reliability of the model was verified. These preliminary studies have achieved the purpose of rapid control of the fire in the whole region of the goaf and provided valuable lessons for similar nitrogen injection fire prevention and extinguishing technologies in goaf.
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References
Alam P, Siddiqui NA, Rehman MT, Hussain A, Akhtar A, Mir SR, Alajmi MF (2021) Box-Behnken design (BBD)-based optimization of microwave-assisted extraction of parthenolide from the stems of Tarconanthus camphoratus and cytotoxic analysis. Molecules 26:1876
Bas D, Boyaci IH (2007) Modeling and optimization I: usability of response surface methodology. J Food Eng 78:836–845
Box GEP, Behnken DW (1960) Some new three level designs for the study of quantitative variables. Technometrics 2:455–475
Chakawa S, Aziz M (2021) Investigating the result of current density, temperature, and electrolyte concentration on COD: subtraction of petroleum refinery wastewater using response surface methodology. Water-Sui 13:835
Chaker H, Ameur N, Saidi-Bendahou K, Djennas M, Fourmentin S (2021) Modeling and Box-Behnken design optimization of photocatalytic parameters for efficient removal of dye by lanthanum-doped mesoporous TiO2. J Environ Chem Eng 9:104584
Deng J, Yang Y, Zhang YN, Liu B, Shu CM (2018) Inhibiting effects of three commercial inhibitors in spontaneous coal combustion. Energy 160:1174–1185
Frey DD, Sudarsanarn M (2008) An adaptive one-factor-at-a-time method for robust parameter design: comparison with crossed arrays via case studies. J Mech Design 130: 021401
Ghellab SE, Mu W, Li QC, Han XJ (2019) Prediction of the size of electroformed giant unilamellar vesicle using response surface methodology. Biophys Chem 253:106217
Guo XY, Deng CB, Zhang X, Wang YS (2019) Formation law of hydrocarbon index gases during coal spontaneous combustion in an oxygen-poor environment. Energ Source Part A 41:626–635
Hao Y, Xie TP (2021) Coupling treatment of gas drainage and nitrogen injection for fire prevention in the first stratified mining goaf: theoretical calculation and field experiment. Combust Sci Technol 1:1–15
Li ZX, Li J, Li L, Zhao ZJ (2017) Simulation on nitrogen injection for fire preventing in goaf of complex stope based on “two intake and one return airway.” J Liaoning Tech Univ (Nat Sci) 36(8):785–789. https://doi.org/10.11956/j.issn.1008-0562.2017.08.001
Li QW, Xiao Y, Zhong K-Q, Shu C-M, Lü H-F, Deng J, Wu S (2020) Overview of commonly used materials for coal spontaneous combustion prevention. Fuel 275:117981
Liu MX, Shi GQ, Guo ZX, Wang YM, Ma LY (2016) 3-D simulation of gases transport under condition of inert gas injection into goaf. Heat Mass Transfer 52:2723–2734
Lu XX, Zhu HQ, Wang DM, Hu C, Zhao HR, Huo YJ (2018) Flow characteristic investigation of inhibition foam used for fire extinguishment in the underground goaf. Process Saf Environ 116:159–168
Ma C, Yu HH, Gao YJ, Xu WJ, Xu TF, Wang L, Zhao B, Zhang ZH, Xu J (2020) Operation parameters optimization of a hybrid dead-end/cross-flow forward osmosis system for microalgae dewatering by response surface methodology. Process Saf Environ 143:14–24
Markandeya DN, Shukla SP, Kisku GC (2017) Statistical optimization of process parameters for removal of dyes from wastewater on chitosan cenospheres nanocomposite using response surface methodology. J Clean Prod 149:597–606
Nekkaa A, Benaissa A, Lalaouna A, Mutelet F, Canabady-Rochelle L (2021) Optimization of the extraction process of bioactive compounds from Rhamnus alaternus leaves using Box-Behnken experimental design. J Appl Res Med Aroma 25:100345
Ockuly RA, Weese ML, Smucker BJ, Edwards DJ, Chang L (2017) Response surface experiments: a meta-analysis. Chemometr Intell Lab 164:64–75
Pragasam V, Degalahal MR (2020) Investigation on flexural strength of cellulose microfibrils reinforced polymer composite. Emerg Mater Res 9:1–12
Qi QJ (2019) QiY, Zhou XH (2019) Dynamic effects of air supply volume on spontaneous combustion in goafs and fire prevention and extinguishing technology [J]. China Saf Sci J 29(04):120–126. https://doi.org/10.16265/j.cnki.issn1003-3033.2019.04.019
Qi Y, Wang W, Qi Q, Ning Z, Yao Y (2021) Distribution of spontaneous combustion three zones and optimization of nitrogen injection location in the goaf of a fully mechanized top coal caving face. PLoS ONE 16:e0256911
Rahimi M, Valeh-e-Sheyda P, Rashidi H (2017) Statistical optimization of curcumin nanosuspension through liquid anti-solvent precipitation (LASP) process in a microfluidic platform: Box-Behnken design approach. Korean J Chem Eng 34:3017–3027
Sadeghi E, Movagharnejad K, Haghighi Asl A (2019) Mathematical modeling of infrared radiation thin-layer drying of pumpkin samples under natural and forced convection. J Food Proc Preserv 43:14229
Shao ZL, Jia XY, Zhong XX, Wei J, Wang YM, Chen L (2018) Detection, extinguishing, and monitoring of a coal fire in Xinjiang, China. Environ Sci Pollut Res 25:26603–26616
Shao Z, Tan B, Li T, Guo Y, Wang H, Li X, Cheng G, Wang P (2022) Study on oxidation and pyrolysis characteristics of lignite damaged by liquid CO2 at low-temperature. Fuel 323:124371
Shi B, Zhou F (2014) Impact of heat and mass transfer during the transport of nitrogen in coal porous media on coal mine fires. Sci World J 2014:293142
Shi B, Ma L, Dong W, Zhou F (2015) Application of a novel liquid nitrogen control technique for heat stress and fire prevention in underground mines. J Occup Environ Hyg 12:D168–D177
Shi GQ, Px D, Guo Z, Wang Y-m (2019) Modeling temperature distribution upon liquid-nitrogen injection into a self heating coal mine goaf. Process Saf Environ 126:278–286
Song ZY, Kuenzer C (2014) Coal fires in China over the last decade: a comprehensive review. Int J Coal Geol 133:72–99
Song ZY, Kuenzer C (2017) Spectral reflectance (400–2500 nm) properties of coals, adjacent sediments, metamorphic and pyrometamorphic rocks in coal-fire areas: a case study of Wuda coalfield and its surrounding areas, northern China. Int J Coal Geol 171:142–152
Swati, Ghosh P, Thakur IS (2019) Biodegradation of pyrene by Pseudomonas sp. ISTPY2 isolated from landfill soil: process optimisation using Box-Behnken design model. Bioresource Technol Rep 8:100329
Thangam R, Suresh V, Kannan S (2014) Optimized extraction of polysaccharides from Cymbopogon citratus and its biological activities. Int J Biol Macromol 65:415–423
Tian ZJ, Li XL (2012) Research on technology for preventing spontaneous combustion of coal. Nat Resources Sustain Devel Ii Pts 1–4(524–527):677–680
Wang CP, Deng Y, Zhang YT, Xiao Y, Deng J, Shu CM (2022a) Coal oxidation characteristics and index gases of spontaneous combustion during the heating and cooling processes. Fuel 307:121806
Wang W, Qi Y, Liu J (2022b) Study on multi field coupling numerical simulation of nitrogen injection in goaf and fire-fighting technology. Sci Rep 12:17399
Wen H, Liu Y, Guo J, Jin YF, Zheng XZ (2021) A multi-index-classified early warning method for spontaneous combustion of coal under air leakage blocking. J Oil Gas Coal Technol 27:208–226
Xin C, Lu L, Shi B, Zhongxin L (2018) Numerical investigation of local thermal non-equilibrium effects in coal porous media with cryogenic nitrogen injection. Int J Therm Sci 133:32–40
Yang Y, Li Z, Si L, Hou S, Zhou Y, Qi Q (2017) Consolidation grouting technology for fire prevention in mined-out areas of working face with large inclined angle and its application. Fire Mater 41:700–715
Zhang Y, Wu B, Liu SH, Lei BW, Zhao JL, Zhao YT (2020) Thermal kinetics of nitrogen inhibiting spontaneous combustion of secondary oxidation coal and extinguishing effects. Fuel 278:118223
Zhang LD, Song ZY, Wu DJ, Luo ZM, Zhao SS, Wang YH, Deng J (2022) Prediction of coal self-ignition tendency using machine learning. Fuel 325:124832
Zhu HQ, Li F, Gao RL, Jiang YG, Pan FL (2011) Design and traction power calculation of non-interval drag pipe nitrogen injection for fire control. First Int Symp Mine Saf Sci Eng 26:595–601
Zhu HQ, Guo S, Xie YY, Zhao HR (2021) Molecular simulation and experimental studies on CO2 and N2 adsorption to bituminous coal. Environ Sci Pollut Res 28:15673–15686
Zhuo H, Qin B, Qin Q, Su Z (2019) Modeling and simulation of coal spontaneous combustion in a gob of shallow buried coal seams. Process Saf Environ Prot 131:246–254
Funding
This work was supported by the National Natural Science Foundation of China (No.51774290) and the Fundamental Research Funds for Central Universities (2020YQAQ02 and 2020YJSAQ17).
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Hongqing Zhu: investigation, methodology, experiment, data curation, and writing—original draft. Lintao Hu: conceptualization, data curation, funding acquisition, supervision, and writing—review and editing. Baolin Qu: investigation and writing—review and editing. Qi Liao: investigation and writing—review and editing. Chang Tian: investigation and writing—review and editing. Xiaozhen Song: investigation and writing—review and editing. XiYang Fang: investigation and writing—review and editing. Xuedong Zhang: investigation and writing—review and editing.
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Zhu, H., Hu, L., Qu, B. et al. Optimization of key parameters for continuous and precise nitrogen injection in goaf based on response surface methodology. Environ Sci Pollut Res 30, 40189–40205 (2023). https://doi.org/10.1007/s11356-022-25037-7
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DOI: https://doi.org/10.1007/s11356-022-25037-7