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Kinetics of adsorption of poly(vinylimidazole) (PVI) onto copper surfaces investigated by quartz crystal microbalance studies

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Abstract

Organic corrosion inhibitors offer a huge potential of lowering product cost and manufacturing complexity in printed circuit board industry. Up to now, there is no reliable and fast method available to classify materials according to their ability to prevent copper from corrosion based on kinetic data of adsorption. We investigated the potential of the recently presented fast impedance-scanning quartz microbalance (FIS-QCM) to perform such studies. We selected poly(vinylimidazole) (PVI) that is known for its excellent ability to prevent copper from corrosion. However, kinetics and free energy of adsorption of PVI were never investigated. This paper presents the results of these studies. Reliable kinetic data were obtained, and the measurements show also the excellent frequency stability of this device that enables the detection of very small changes in resonance behaviour of the sensor quartz crystal, even below 1 Hz.

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Acknowledgements

This work is dedicated to Professor Waldfried Plieth in celebration of Professor Waldfried Plieth’s 75th Birthday on 7th November 2012. One of us (HJG) cordially thanks Professor Waldfried Plieth for his interest in and support of his work in several fields of electrochemistry and physical chemistry during many years. Financial support from the German Research Foundation (DFG), contract number 544243 (Project Initiative PAK 177 “Funktionsmaterialien und Materialanalytik zu Lithium-Hochleistungsbatterien”) is gratefully acknowledged.

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Authors and Affiliations

  1. Workgroup “Electrochemistry and Electrolytes”, Institute of Physical and Theoretical Chemistry, University of Regensburg, 93040, Regensburg, Germany

    Tobias Simbeck, Michael Maximilian Hammer, Stefan Thomaier & Edmund Riedl

  2. Institute of Physical Chemistry, Münster, Electrochemical Energy Technology (MEET), Westfälische Wilhelms-Universität (WWU) Münster, Corrensstraße 46, 48149, Münster, Germany

    Christoph Stock & Heiner Jakob Gores

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  1. Tobias Simbeck
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  2. Michael Maximilian Hammer
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  3. Stefan Thomaier
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  4. Christoph Stock
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  5. Edmund Riedl
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  6. Heiner Jakob Gores
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Correspondence to Heiner Jakob Gores.

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Simbeck, T., Hammer, M.M., Thomaier, S. et al. Kinetics of adsorption of poly(vinylimidazole) (PVI) onto copper surfaces investigated by quartz crystal microbalance studies. J Solid State Electrochem 16, 3467–3472 (2012). https://doi.org/10.1007/s10008-012-1838-9

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  • DOI: https://doi.org/10.1007/s10008-012-1838-9

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