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Precipitation and dissolution behaviors of δ phase inside a deformed nickel-based superalloy during annealing treatment

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Abstract

The precipitation and dissolution behaviors of δ phase inside a deformed nickel-based superalloy during annealing treatment are investigated. A new method for quantitatively evaluating the content of δ phase was proposed based on SEM micrograph, which was verified by X-ray diffraction (XRD) analysis. The effects of recrystallization during pre-annealing at 980 °C on the precipitation and dissolution behaviors of δ phase in the subsequent annealing treatment at 900 °C and 980 °C are discussed. Moreover, the improved precipitation and dissolution kinetics models are proposed to consider the effects of recrystallization fraction. The results show that: (1) for the precipitation of δ phase at 900 °C, δ phases precipitate first in grain boundaries and then within grains after a long incubation period. Moreover, the interval between adjacent δ phases increases first and then drops with the increasing recrystallization fraction during pre-annealing treatment. A balance between the precipitation and solution of δ phase at the aging temperature of 900 °C can be reached when the holding time is about 12 h; (2) for the dissolution of δ phase at 980 °C, the dissolution equilibrium can be obtained at approximate 200 min. Moreover, more rod-like δ phases can be remained with the increasing recrystallization fraction in pre-annealing treatment.

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Acknowledgements

This work was supported by National Natural Science Foundation of China (no. 51775564), the Science and Technology Leading Talent in Hunan Province (no. 2016RS2006), Program of Chang Jiang Scholars of Ministry of Education (no. Q2015140), the Open-End Fund for the Valuable and Precision Instruments of Central South University (no. CSUZC201920), and the Foundation of Educational Commission of Hebei Province of China (no. QN2019051).

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Authors and Affiliations

  1. School of Mechanical and Electrical Engineering, Central South University, Changsha, 410083, China

    Ming-Song Chen, Guan-Qiang Wang, Hong-Bin Li, Y. C. Lin, Zong-Huai Zou, Yan-Yong Ma, Dao-Guang He & Wei-Dong Zeng

  2. Light Alloy Research Institute of Central South University, Changsha, 410083, China

    Ming-Song Chen, Y. C. Lin & Dao-Guang He

  3. State Key Laboratory of High Performance Complex Manufacturing, Changsha, 410083, China

    Guan-Qiang Wang, Y. C. Lin, Zong-Huai Zou, Yan-Yong Ma & Wei-Dong Zeng

  4. College of Metallurgies and Energy, North China Science and Technologies University, Tangshan, 063009, China

    Hong-Bin Li

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Chen, MS., Wang, GQ., Li, HB. et al. Precipitation and dissolution behaviors of δ phase inside a deformed nickel-based superalloy during annealing treatment. Appl. Phys. A 125, 447 (2019). https://doi.org/10.1007/s00339-019-2741-3

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