Abstract
Purpose
To evaluate bonding quality for orthodontic bracket bonding with different component combinations of self-etch primers in vitro.
Methods
Metallic brackets were bonded to bovine lower incisors and assigned to groups. Group 1: comparison of self-etch (Transbond™ Plus, 3M™ Unitek, Neuss, Germany, n = 30; BrackFix® primer SE, VOCO®, Cuxhaven, Germany, n = 20) and etch-and-rinse bonding systems (Transbond™ XT, n = 20; BrackFix®, n = 20); group 2: comparison of different self-etch primer (Transbond™ Plus; BrackFix® primer SE) and adhesive (Transbond™ XT, n = 20; BrackFix®, n = 20) product combinations; group 3: testing cyclic fatigue bond strength of self-etch bonding systems (Transbond™ Plus, n = 20; BrackFix® primer SE, n = 20). All teeth were tested for shear bond strength according to the DIN-13990 standard, the adhesive remnant index (ARI) and enamel fractures were determined microscopically (10 × magnification).
Results
The mean shear bond strength of the self-etch (Transbond™ Plus: 16.38 ± 3.68 MPa; BrackFix® primer SE: 16.24 ± 1.73 MPa) and etch-and-rinse bonding systems (Transbond™ XT: 18.45 ± 2.56 MPa; BrackFix®: 17 ± 5.2 MPa) were of a clinically adequate order of magnitude (≥ 6–10 MPa) and were not statistically different. The component combination BrackFix® primer SE/Transbond™ XT adhesive led to a significantly lower shear bond strength (11.99 ± 3.68 MPa). There were no significant differences between static and fatigue shear bond strengths of self-etch bonding systems. Mean ARI scores mostly ranged between 4 and 5. The combination of the self-etch primer Transbond™ Plus with the BrackFix® adhesive led to a significantly increased enamel fracture rate.
Conclusions
Based on the present findings bond strength of self-etch primers was equal to etch-and-rinse primers for bracket bonding. Combining different self-etch bonding systems might alter the clinical performance.
Zusammenfassung
Zielsetzung
In-vitro-Evaluation, ob die Kombination verschiedener selbstätzender Bondingsysteme die Verbundqualität bei der Bracketbefestigung beeinflusst.
Methode
Metallbrackets wurden auf bovinen Zähnen befestigt und in Gruppen aufgeteilt. Gruppe 1: Vergleich selbstätzender Primer-Adhäsiv-Gemische (Transbond™ Plus, 3M™ Unitek, Neuss, Deutschland; n = 30; BrackFix® primer SE, VOCO®, Cuxhaven, Deutschland, n = 20) mit konventionellen Säure-Ätz-Techniken (Transbond™ XT, n = 20; BrackFix®, n = 20); Gruppe 2: Kombination selbstätzender Primer (Transbond™ Plus; BrackFix® primer SE) mit Adhäsiven anderer Hersteller (Transbond™ XT, n = 20; BrackFix®, n = 20); Gruppe 3: Untersuchung selbstätzender Bondingsysteme (Transbond™ Plus, n = 20; BrackFix® primer SE, n = 20) unter zyklischer Dauerbelastung. Alle Proben wurden hinsichtlich der Scherhaftfestigkeit nach DIN-13990 geprüft sowie der ARI („adhesive remnant index“) und Schmelzausrisse mikroskopisch bestimmt (10-fache Vergrößerung).
Ergebnisse
Die Verbundhaftfestigkeiten selbstätzender (Transbond™ Plus: 16,38 ± 3,68 MPa; BrackFix® primer SE: 16,24 ± 1,73 MPa) und konventioneller Bondingsysteme (Transbond™ XT: 18,45 ± 2,56 MPa; BrackFix®: 17 ± 5,2 MPa) lagen in einem klinisch akzeptablen Bereich (≥6–10 MPa) und zeigten keine statistisch signifikanten Unterschiede. Die Kombination von Primern und Adhäsiven unterschiedlicher Hersteller führte in der Kombination BrackFix® primer SE/Transbond™ XT Adhäsiv (11,99 ± 3,68 MPa) zu einer signifikant verringerten Verbundqualität. Es lagen keine Unterschiede zwischen statischer und zyklischer Verbundhaftfestigkeit selbstätzender Bondingsysteme vor. Die durchschnittlichen ARI-Scores lagen überwiegend zwischen 4 and 5. Die Kombination von Transbond™ Plus Primer/BrackFix® Adhäsiv führte zu einer signifikant höheren Schmelzfrakturrate.
Schlussfolgerung
Die Verbundqualität selbstätzender und konventioneller Bondingsysteme zeigte sich gleichwertig. Die Kombination unterschiedlicher Primer- und Adhäsivkomponenten kann die klinische Performance verändern.
Access this article
We’re sorry, something doesn't seem to be working properly.
Please try refreshing the page. If that doesn't work, please contact support so we can address the problem.
Similar content being viewed by others
Abbreviations
- ARI:
-
Adhesive remnant index
References
Diedrich P (1981) Die Verbundfestigkeit verschiedener orthodontischer Adhäsive zum konditionierten Schmelz und zur Bracketbasis. Fortschr Kieferorthop 42:305–320
Reynolds I (1974) A review of direct orthodontic bonding. Br J Orthod 2:171–178
Stasinopoulos D, Papageorgiou SN, Kirsch F et al (2018) Failure patterns of different bracket systems and their influence on treatment duration: a retrospective cohort study. Angle Orthod 88:338–347. https://doi.org/10.2319/081817-559.1
Linklater RA, Gordon PH (2001) An ex vivo study to investigate bond strengths of different tooth types. J Orthod 28:59–65. https://doi.org/10.1093/ortho/28.1.59
Bishara SE, VonWald L, Laffoon JF, Warren JJ (2000) The effect of repeated bonding on the shear bond strength of different orthodontic adhesives. Angle Orthod 70:435–441. https://doi.org/10.1067/mod.2002.123042
Edwards D, Berry JJ (1987) The efficiency of simulation-based multiple comparisons. Biometrics 43:913–928
Buonocore M (1955) A simple method of increasing the adhesion of acrylic filling materials to enamel surfaces. J Dent Res 34:849–853
Mandall N, Millett D, Mattick C et al (2003) Adhesives for fixed orthodontic brackets. Cochrane Database Syst Rev 2:CD2282
Sunna S, Rock W (1998) Clinical performance of orthodontic brackets and adhesive systems: a randomized clinical trial. Br J Orthod 25:283–287
Gottlieb E, Retief D, Jamison H (1982) An optimal concentration of phosphoric acid as an etching agent. Part I: tensile bond strength studies. J Prosthet Dent 48:48–51
Ohsawa T (1972) Studies on solubility and adhesion of the enamel in pre-treatment for caries preventive sealing. Bull Tokyo Dent Coll 13:65–82
Carstensen W (1992) The effects of different phosphoric acid concentrations on surface enamel. Angle Orthod 62:51–58
Wang W, Lu T (1991) Bond strength with various etching times on young permanent teeth. Am J Orthod Dentofacial Orthop 100:72–79
Sadowsky P, Retief D, Cox P et al (1990) Effects of etchant concentration and duration on the retention of orthodontic brackets: an in vivo study. Am J Orthod Dentofacial Orthop 98:417–421. https://doi.org/10.1016/S0889-5406(05)81650-6
Kinch A, Taylor H, Warltier R et al (1989) A clinical study of amount of adhesive remaining on enamel after debonding, comparing etch times of 15 and 60 seconds. Am J Orthod Dentofacial Orthop 95:415–421. https://doi.org/10.1016/0889-5406(89)90303-x
Carstensen W (1986) Clinical results after direct bonding of brackets using shorter etching times. Am J Orthod 89:70–72. https://doi.org/10.1016/0002-9416(86)90114-4
Hu H, Li C, Chen J et al (2013) Enamel etching for bonding fixed orthodontic braces. Cochrane Database Syst Rev 11:CD5516. https://doi.org/10.1002/14651858.CD005516.pub2
Fleming P, Johal A, Pandis N (2012) Self-etch primers and conventional acid-etch technique for orthodontic bonding: a systematic review and meta-analysis. Am J Orthod Dentofacial Orthop 142:83–94. https://doi.org/10.1016/j.ajodo.2012.02.023
Giannini M, Makishi P, Ayres A et al (2015) Self-etch adhesive systems: a literature review. Braz Dent J 26:3–10. https://doi.org/10.1590/0103-6440201302442
Wang Y, Spencer P (2004) Physiochemical interactions at the interfaces between self-etch adhesive systems and dentine. J Dent 32:118–132
Van Landuyt K, Snauwaert J, De Munck J et al (2007) Systematic review of the chemical composition of contemporary dental adhesives. Biomaterials 28:3757–3785
Yoshida Y, Nagakane K, Fukuda R et al (2004) Comparative study on adhesive performance offunctional monomers. J Dent Res 83:454–458
Knaup I, Böddeker A, Tempel K et al (2020) Analysing the potential of hydrophilic adhesive systems to optimise orthodontic bracket rebonding. Head Face Med 16:20. https://doi.org/10.1186/s13005-020-00233-3
Knaup T, Korbmacher-Steiner H, Braun A et al (2020) Effects of 445-nm diode laser-assisted debonding of metallic brackets on shear bond strength and enamel surface morphology. Photobiomodul Photomed Laser Surg 38:160–166. https://doi.org/10.1089/photob.2019.4704
Daratsianos N, Schütz B, Reimann S et al (2019) The influence of enamel sandblasting on the shear bond strength and fractography of the bracket-adhesive-enamel complex tested in vitro by the DIN 13990:2017-04 standard. Clin Oral Investig 23:2975–2985. https://doi.org/10.1007/s00784-018-2692-7
Dixon W, Mood A (1948) A method for obtaining and analyzing sensitivity data. J Am Stat Assoc 43:109–126
Deutsches Institut für Normung e. V. (2017) DIN 13990:2017-04, dentistry—testmethods for shear bond strength of adhesives for orthodontic attachments
Bishara S, Trulove T (1990) Comparisons of different debonding techniques for ceramic brackets: an in vitro study. Part II. Findings and clinical implications. Am J Orthod Dentofacial Orthop 98:263–273
Ibrahim A, Al-Hasani N, Thompson V, Deb S (2020) In vitro bond strengths post thermal and fatigue load cycling of sapphire brackets bonded with self-etch primer and evaluation of enamel damage. J Clin Exp Dent 12:e22–e30. https://doi.org/10.4317/medoral.56444
Imani M, Aghajani F, Momeni N, Akhoundi M (2018) Effect of cyclic loading on shear bond strength of orthodontic brackets: an in vitro study. J Dent 15:351–357
Schauseil M, Blöcher S, Hellak A et al (2016) Shear bond strength and debonding characteristics of a new premixed self-etching with a reference total-etch adhesive. Head Face Med 12:19. https://doi.org/10.1186/s13005-016-0117-x
Farhadian N, Miresmaeili A, Zandi V (2019) Shear bond strength of brackets bonded with self-etching primers compared to conventional acid-etch technique: a randomized clinical trial. Front Dent 16:248–255. https://doi.org/10.18502/fid.v16i4.2083
Kim YK, Park H‑S, Kim K‑H, Kwon T‑Y (2015) Effect of adhesive resin flexibility on enamel fracture during metal bracket debonding: an ex vivo study. Eur J Orthod 37:550–555. https://doi.org/10.1093/ejo/cju086
Daratsianos N, Musabegovic E, Reimann S et al (2013) The influence of cyclic shear fatigue on the bracket-adhesive-enamel complex: an in vitro study. Dent Mater 29:506–513. https://doi.org/10.1016/j.dental.2013.01.003
Algera TJ, Kleverlaan CJ, Prahl-Andersen B, Feilzer AJ (2008) The influence of dynamic fatigue loading on the separate components of the bracket-cement-enamel system. Am J Dent 21:239–243
BenGassem A, Georgiou G, Jones S (2013) Initial and fatigue bond strengths of nanofilled and conventional composite bonding adhesives. J Orthod 40:137–144. https://doi.org/10.1179/1465313312Y.0000000034
Hajrassie M, Khier S (2007) In-vivo and in-vitro comparison of bond strengths of orthodontic brackets bonded to enamel and debonded at various times. Am J Orthod Dentofacial Orthop 131:384–390
Pickett K, Sadowsky P, Jacobson A, Lacefield W (2001) Orthodontic in vivo bond strength: comparison with in vitro results. Angle Orthod 71:141–148
Eliades T, Bourauel C (2005) Intraoral aging of orthodontic materials: the picture we miss and its clinical relevance. Am J Orthod Dentofacial Orthop 127:403–412
Acknowledgements
The authors thank the Otto Schott Institute of Materials Research, University of Jena, Germany and the Medical Faculties of Jena and Aachen, Germany for scientific support.
Funding
The study was funded by the companies VOCO® GmbH, Cuxhaven, Germany, which was involved in financial and material support, DENTAURUM GmbH & Co. KG, Ispringen, Germany and 3M Unitek GmbH, Neuss, Germany, which were involved in material support. None of the mentioned companies were involved in either data collection, analysis and interpretation or writing of the article.
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
Conflict of interest
I. Knaup, E. Weber, A. Böddeker, K. Tempel, M.V. Rückbeil, J.R. Bartz, A. Bastian, Y. Wagner and M. Wolf declare that they have no competing interests.
Ethical standards
This article does not report on any studies with human participants or animals that were performed by any of the authors.
Additional information
Publisher’s Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Knaup, I., Weber, E., Böddeker, A. et al. Effect of using different component combinations for orthodontic bracket bonding with self-etch primers. J Orofac Orthop 84 (Suppl 2), 84–92 (2023). https://doi.org/10.1007/s00056-021-00356-5
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s00056-021-00356-5