Abstract
Microwave-assisted extraction (MAE) was developed for the fast extraction of solanesol from potato leaves and stems. The ratio of raw material to ethanol, extraction time, extraction temperature, and microwave irradiation power were interdependent. The yield of solanesol reached its maximum 98.57% with 1:8.0 g/ml, 40 min, 55°C, and 2.0 KW, respectively. MAE was comparable to other extraction methods, including solvent extraction, heat-reflux, and Soxhlet-extraction. MAE reduced extraction time, solvent consumption, and increased yields of solanesol. Solanesol concentration was performed by RP-high performance liquid chromatography. The method was rapid, simple, accurate, and reproducible.
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References
Akhter MH, Croteau LG (1996) Extraction of salinomycin from finished layers ration by microwave solvent extraction followed by liquid chromatography. Analyst (Lond) 121(6):803–806. doi:10.1039/AN9962100803
Asahina M, Kato H, Fukawah H (1977) Process for the manufacture of solanesol. [P].US:4013731
Chena JH, Liu XP, Xu XQ, Lee FSC, Wang XR (2007) Rapid determination of total solanesol in tobacco leaf by ultrasound-assisted extraction with RP-HPLC and ESI-TOF/MS. J Pharm Biomed 43:879–885. doi:10.1016/j.jpba.2006.09.003
Greenway GM, Kometa N (1994) On-line sample preparation for the determination of riboflavin and flavin mononucleotides in food stuffs. Analyst (Lond) 119(5):929–935. doi:10.1039/an9941900929
Hamamura K, Yamatsu I, Minami N, Yamagishi Y, Inai Y, Kijima S, Nakamura T (2002) Synthesis of [3–14C] coenzyme Q10. J Labelled Comp Radiopharm 45:823–829. doi:10.1002/jlcr.588
Judy WV, Hall JH, Toth PD, Folkers K (1986) Long-term management of end-stage heart failure with coenzyme Q10. In: Folkers K, Yamamura Y (eds) Biomedical and clinical aspects of coenzyme Q10, vol 5. Elsevier Science, Amsterdam, pp 291–301
Lenaz G, Espoli MD (1985) Physical properties of ubiquinone in model systems and membranes. In: Lenaz G (ed) Coenzyme Q: biochemistry, bioenergetics and clinical applications of ubiquinone. John Wiley, New York, pp 83–106
Pan YM, Wang K, Huang SQ et al (2008) Antioxidant activity of microwave-assisted extract of longan (Dimocarpus Longan Lour.) peel. Food Chem 106:1264–1270. doi:10.1016/j.foodchem.2007.07.033
Rowland RL, Latimer PH, Giles JA (1956) Flue-cured I. Tobacco, isolation of solanesol, an unsaturated ethanol. J Am Chem Soc 78(18):4680–4683. doi:10.1021/ja01599a041
Takemura M, Amano M (1979) Method of gathering solanesol. [P].JP:54138510
Tao YH, Ren ZY, Liu GQ (2002) Extract and quantitation determination of solanesol from discarded tobacco in Yunnan province. J Yunnan Univ Nat Sci 24(2):151
Wang YW, Bonilla M, Mcnain HM (1997) Solid-phase microextracion associated with microwave assisted extraction of food products. J High Resolut Chromatogr 20:213–216
Wang YT, You JY, Yu Y et al (2008) Analysis of ginsenosides in Panax ginseng in high pressure microwave-assisted extraction. Food Chem 110:161–167. doi:10.1016/j.foodchem.2008.01.028
Wieteska E, Ziock A (1996) Extraction as a method for preparation of vegetable samples for the determination of trace metals by atomic absorption spectrometry. Anal Chim Acta 330:251–257. doi:10.1016/0003-2670(96)00187-0
Zhang MS, Li JX (2001) Determination of solanesol in the extracts of tobacco leaves by high performance liquid chromatography. Chin J Chromatogr 19(5):470
Zhao CJ, Li CY, Zu YG (2007) Rapid and quantitative determination of solanesol in Nicotiana tabacum by liquid chromatography–tandem mass spectrometry. J Pharm Biomed 44:35–40. doi:10.1016/j.jpba.2007.01.021
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Chen, T., Sun, X., Xiao, W. et al. Optimization of microwave-assisted extraction of solanesol from potato leaves and stems. Med Chem Res 19, 732–742 (2010). https://doi.org/10.1007/s00044-009-9226-4
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DOI: https://doi.org/10.1007/s00044-009-9226-4