Summary
The separation of β-pinene and menthone by HPLC on a silica gel column can be significantly improved with decreasing the column temperature. On a perparative scale complete separation of oxygenated terpenes from terpene hydrocarbons could be carried out under such conditions.
References
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Yamasaki, T., Sakai, M., Kanamori, T. et al. Low temperature liquid chromatographic separation of oxygenated terpenes from terpene hydrocarbons. Chromatographia 21, 478–479 (1986). https://doi.org/10.1007/BF02341274
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DOI: https://doi.org/10.1007/BF02341274