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Über Synthese und Strukturbeweis von substituierten 5-Phenyl-1H-thieno[3,4—e]1,4-diazepin-2(3H)-onen

Synthesis and proof of structure of substituted 5-Phenyl-1H-thieno[3.4—e]1.4-diazepin-2(3H)-ones

  • Organische Chemie und Biochemie
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Abstract

Chlorination and nitration of 5-phenyl-1H-thieno-[3.4-e]1.4-diazepin-2(3H)-one (1) are described. It is proved by unambiguous synthesis of the chloro derivative that electrophilic substitution of1 occurs in position 8. Chlorinated1 is methylated in position 1.

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Literatur

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Hromatka, O., Binder, D. & Eichinger, K. Über Synthese und Strukturbeweis von substituierten 5-Phenyl-1H-thieno[3,4—e]1,4-diazepin-2(3H)-onen. Monatshefte für Chemie 104, 1599–1606 (1973). https://doi.org/10.1007/BF00909646

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  • DOI: https://doi.org/10.1007/BF00909646

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