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Nuclear Magnetic Resonance Spectroscopy of Cement-Based Materials

  • Conference proceedings
  • © 1998

Overview

Editors:
  1. Pierre Colombet

    1. CTG Italcementi-Ciments Français, Guerville, France

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  2. Hélène Zanni

    1. ESPCI, Paris Cedex 5, France

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  3. Arnd-Rüdiger Grimmer

    1. Institut für Chemie, Humboldt-Universität, Germany

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  4. Piero Sozzani

    1. Dipartimento di Scienza dei Materiali, Chimica e Technologia dei Materiali, Universita degli Studi di Milano, Milano, Italy

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Table of contents (36 papers)

  1. Front Matter

    Pages I-XV
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  2. Clinkerization Reactions and Anhydrous Phase Characterization

    1. Front Matter

      Pages 1-1
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    2. Characterization of the Calcium Silicate and Aluminate Phases in Anhydrous and Hydrated Portland Cements by 27Al and 29Si MAS NMR Spectroscopy

      • Jørgen Skibsted, Hans J. Jakobsen
      Pages 3-45

    3. In Situ High Temperature Multinuclear NMR Study of Clinker Formation

      • Laurent Bonafous, Catherine Bessada, Dominique Massiot, Jean-Pierre Coutures, Bruno LeRolland, Pierre Colombet
      Pages 47-55

    4. 29Si NMR Study of Chemical Shift Tensor Anisotropy of Tricalcium Silicate

      • Arnd-Rüdiger Grimmer, Hélène Zanni
      Pages 57-68

    5. Relationship between NMR 29Si Chemical Shifts and FT-IR Wave Numbers in Calcium Silicates

      • Yoshihiko Okada, Tsuguya Masuda, Minori Takada, Lingling Xu, Takeshi Mitsuda
      Pages 69-78

    6. Multiquantum (3Q and 5Q) MAS NMR Spectroscopy of Aluminium-27 in Solids

      • C. Fernandez, J. P. Amoureux, Y. Dumazy, L. Delevoye
      Pages 79-88

    7. New Progress in High Resolution 27Al and 17O Solid State NMR (MAS and MQ-MAS) of Aluminium Bearing Phases

      • Dominique Massiot, Bruno Touzo, Dominique Trumeau, Claire Magnenet, Valérie Montouillout, Pierre Florian et al.
      Pages 89-105

    8. Time Resolved Very High Temperature NMR Study of the Cooling Process of CaO-Al2O3 Liquids

      • Dominique Massiot, Bruno Touzo, Dominique Trumeau, Ian Farnan, Jean-Claude Rifflet, Catherine Bessada et al.
      Pages 107-116

  3. The Nanostructure of C-S-H

    1. Front Matter

      Pages 117-117
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    2. C-S-H Structure Evolution with Calcium Content by Multinuclear NMR

      • Ivan Klur, Benoît Pollet, Joseph Virlet, André Nonat
      Pages 119-141

    3. The Structure of Calcium Silicate Hydrate: NMR and Raman Spectroscopic Results

      • Xiandong Cong, R. James Kirkpatrick, Jeffrey L. Yarger, Paul F. McMillan
      Pages 143-158

    4. 29Si MAS NMR Spectroscopy of Poorly-Crystalline Calcium Silicate Hydrates (C-S-H)

      • Hiroaki Noma, Yoshio Adachi, Hideo Yamada, Tadashi Nishino, Yoshihisa Matsuda, Takushi Yokoyama
      Pages 159-168

    5. Characterization of Protons in C-S-H Phases by Means of High-Speed 1H MAS NMR Investigations

      • Detlef Heidemann, Wolfgang Wieker
      Pages 169-180

    6. Structural Investigation of Calcium Silicate Hydrates by X-Ray Absorption Spectroscopy

      • Nicolas Lequeux, Nathalie Richard
      Pages 181-188

    7. NMR and Infrared Spectroscopies of C-S-H and Al-Substituted C-S-H Synthesised in Alkaline Solutions

      • Isabelle Lognot, Ivan Klur, André Nonat
      Pages 189-196

    8. The Structure, Stoichiometry and Properties of C-S-H Prepared by C3S Hydration Under Controlled Condition

      • André Nonat, Xavier Lecoq
      Pages 197-207

    9. Tricalcium Silicate Hydration at High Temperature. A 29Si and 1H NMR Investigation

      • B. Bresson, S. Masse, H. Zanni, C. Noik
      Pages 209-215

    10. Influence of Heat Treatment Kinetics on Calcium Silicate Hydrates Phase Evolution

      • M.-P. Faugère, M. Crespin, P. Dion, F. Bergaya, A. Feylessoufi, H. Van Damme
      Pages 217-225

    11. Thermochemical and Macromolecular Approach of the C-S-H Structure

      • Roger Dron, Vincent Waller
      Pages 227-234
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Keywords

About this book

NMR spectroscopy has become one of the most powerful methods for the study of the structure and dynamics of solid-state materials. NMR has thus become an important tool, not only in the study of existent cements, but also in the development of new cement-based materials. This volume, based on the proceedings of the second international conference on the NMR Spectroscopy of Cement Based Materials held in Bergamo, Italy, in June 1996, presents the only international overview of the state of the art in the use of NMR in the study of cement-based materials. - This book is of particular interest to all those working in the areas of cement science, material science, solid state chemsitry, analytical chemistry, spectroscopy and those areas of physics engaged in the study of materials.

Editors and Affiliations

  • CTG Italcementi-Ciments Français, Guerville, France

    Pierre Colombet

  • ESPCI, Paris Cedex 5, France

    Hélène Zanni

  • Institut für Chemie, Humboldt-Universität, Germany

    Arnd-Rüdiger Grimmer

  • Dipartimento di Scienza dei Materiali, Chimica e Technologia dei Materiali, Universita degli Studi di Milano, Milano, Italy

    Piero Sozzani

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