Abstract
Additive manufacturing (AM) of Ni-based superalloys such as Alloy 718 may obviate the need for difficult machining and welding operations associated with geometrically intricate parts, thus potentially expanding design possibilities and facilitating cost-effective manufacture of complex components. However, processing AM builds completely free from defects , which may impair mechanical properties such as fatigue and ductility, is challenging. Anisotropic properties, microstructural heterogeneities and local formation of undesired phases are additional concerns that have motivated post-treatment of AM builds. This work investigates the microstructural changes associated with post-treatment of Alloy 718 specimens produced by Electron Beam Melting (EBM ) for as-built microstructures at 3 build heights: near base plate, in the middle of build and near the top of the build. Two different post-treatment conditions, hot isostatic pressing (HIP ) alone and a combined HIP with solutionising and two-step aging were examined and compared to the results for the as-built condition. The influence of various post-treatments on minor phase distributions (δ , γ″, carbides), overall porosity, longitudinal grain widths and Vickers microhardness was considered. The HIP treatment led to significant reduction in overall porosity and dissolution of δ phase, which led to appreciable grain growth for both post-treatment conditions. The variation in hardness noted as a function of build height for the as-built specimens was eliminated after post-treatment . Overall, the hardness was found to decrease after HIP and increase after the full HIP , solutionising and aging treatment, which was attributed to dissolution of γ″ during HIP and its re-precipitation in subsequent heat treatment steps.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
References
Fencheng L, Xin L, Menghua S, Weiwei Z, Jing C, Weidong H (2011) Effect of intermediate heat treatment temperature on microstructure and notch sensitivity of laser solid formed Inconel 718 superalloy. J Wuhan Univ Technol Mater Sci Ed 26(5):908–913
Zhong C, Gasser A, Kittel J, Wissenbach K, Poprawe R (2016) Improvement of material performance of Inconel 718 formed by high deposition-rate laser metal deposition. Mater Des 98:128–134
Strößner J, Terock M, Glatzel U (2015) Mechanical and microstructural investigation of nickel-based superalloy IN718 manufactured by selective laser melting (SLM). Adv Eng Mater 17(8):1099–1105
Sames WJ, Unocic KA, Dehoff RR, Lolla T, Babu SS (2014) Thermal effects on microstructural heterogeneity of Inconel 718 materials fabricated by electron beam melting. J Mater Res 29(17):1920–1930
Gong X, Anderson T, Chou K (2014) Review on powder—based electron beam additive manufacturing technology. Manuf Rev 1(2)
Sochalski-Kolbus LM, Payzant EA, Cornwell PA, Watkins TR, Babu SS, Dehoff RR, Lorenz M, Ovchinnikova O, Duty C (2015) Comparison of residual stresses in Inconel 718 simple parts made by electron beam melting and direct laser metal sintering. Metall Mater Trans A 46(3):1419–1432
Schirra JJ (1997) Development of a improved heat treatment for investment cast Inconel 718 (PWA 649). Paper presented at the superalloys 718,625,706 and various derivatives, Pittsburgh, Pennsylvania, 15–18 June 1997
Anderson M, Thielin AL, Bridier F, Bocher P, Savoie J (2017) δ phase precipitation in Inconel 718 and associated mechanical properties. Mater Sci Eng, A 679:48–55
Siereveld P, Radavich JF, Kelly T, Cole G, Widmer R (1988) Effect of HIP parameters on fine grain cast alloy 718. In: Superalloys, the minerals, metals and materials society, Champion, PA, pp 459–467
Strondl A, Palm M, Gnauk J, Frommeyer G (2011) Microstructure and mechanical properties of nickel based superalloy IN718 produced by rapid prototyping with electron beam melting (EBM). Mater Sci Technol 27(5):876–883
Kirka MM, Medina F, Dehoff R, Okello A (2017) Mechanical behavior of post-processed Inconel 718 manufactured through the electron beam melting process. Mater Sci Eng, A 680:338–346
Deng D, Moverare J, Peng RL, Söderberg H (2017) Microstructure and anisotropic mechanical properties of EBM manufactured Inconel 718 and effects of post heat treatments. Mater Sci Eng, A 693:151–163
Deng D, Saarimä J, Sö H (2016) Microstructural characterization of as-manufactured and heat treated electron beam melted inconel 718. Paper presented at the materials science and technology, Salt Lake City, UT 24–26 Oct 2016
Pröbstle M, Neumeier S, Hopfenmüller J, Freunda LP, Niendorf T, Schwarze D, Göken M (2016) Superior creep strength of a nickel-based superalloy produced by selective laser melting. Mater Sci Eng, A 674:299–307
Sundararaman M, Mukhopadhyay P, Banerjee S (1994) Precipitation and room temperature deformation behaviour of Inconel 718. Paper presented at the superalloys 718, 625, 706 and various derivatives, Pittsburgh, Pennsylvania, 27–29 June 1994
Kirka MM, Greeley DA, Hawkins C, Dehoff RR (2017) Effect of anisotropy and texture on the low cycle fatigue behavior of Inconel 718 processed via electron beam melting. Int J Fatigue 105:235–243
ASTM E1245-03 (2008) Standard practice for determining the inclusion or second-phase constituent content of metals by automatic image analysis
ASTM E562-11 (2011) Standard test method for determining volume fraction by systematic manual point count
Helmer HE, Körner C, Singer RF (2014) Additive manufacturing of nickel-based superalloy Inconel 718 by selective electron beam melting: Processing window and microstructure. J Mater Res 29(17):1987–1996
Sames WJ, Medina F, Peter WH, Babu SS, Dehoff RR (2014) Effect of process control and powder quality on inconel 718 produced using electron beam melting. Paper presented at the 8th international symposium on superalloy 718 and derivatives, Pittsburgh, Pennsylvania, 28 Sept–1 Oct 2014
Mitchell A, Schmalz AJ, Schvezov C, Cockcroft SL (1994) The precipitation of primary carbides in alloy 718. Paper presented at the superalloys 718, 625, 706 and various derivatives, Pittsburgh, Pennsylvania, 27–29 June 1994
Mitchell A (2010) Primary carbides in Alloy 718. Paper presented at the 7th international symposium on superalloy 718 and derivatives, Pittsburgh, Pennsylvania, 10–13 Oct 2010
Belan J (2017) The influence of applied heat-treatment on in 718 fatigue life at three point flexural bending. Metallurgy 56(1–2):167–170
Yun Z, Xuebing H, Yong W, Weicheng Y, Zhuangqi H (1997) Delta phase and deformation fracture behaviour of Inconel 718 alloy. Paper presented at the superalloys 718, 625, 706 and various derivatives, Pittsburgh, Pennsylvania, 15–18 June 1997
Jamshidinia M, Kong F, Kovacevic R (2013) Numerical modeling of heat distribution in the electron beam melting® of Ti-6Al-4V. J Manuf Sci Eng 135(6):061010
Frank RB, Roberts CG, Zhang J (2010) Effect of nickel content on delta solvus temperature and mechanical properties of alloy 718. Paper presented at the 7th international symposium on superalloy 718 and derivatives, Pittsburgh, Pennsylvania, 10–13 Oct 2010
Oradei-Basile A, Radavich JF (1991) A current T-T-T diagram for wrought alloy 718. Paper presented at the superalloy 718, 625 and various derivatives, Pittsburgh, Pennsylvania, 23–26 June 1991
Kuo CM, Yang YT, Bor HY, Wei CN, Tai CC (2009) Aging effects on the microstructure and creep behavior of Inconel 718 superalloy. Mater Sci Eng, A 510–511:289–294
SAE Aerospace (2009) Aerospace material specification: AMS5662
Cai D, Zhang W, Nie P, Liu W, Yao M (2007) Dissolution kinetics of δ phase and its influence on the notch sensitivity of Inconel 718. Mater Charact 58(3):220–225
Niang A, Viguier B, Lacaze J (2010) Some features of anisothermal solid-state transformations in alloy 718. Mater Charact 61:525–534
Raghavan S, Zhang B, Wang P, Sun C-N, Nai MLS, Li T, Wei J (2016) Effect of different heat treatments on the microstructure and mechanical properties in selective laser melted INCONEL 718 alloy. Mater Manuf Process 0(0):1–8
Amato KN, Gaytan SM, Murr LE, Martinez E, Shindo PW, Hernandez J, Collins S, Medina F (2012) Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting. Acta Mater 60(5):2229–2239
Strondl A, Fischer R, Frommeyer G, Schneider A (2008) Investigations of MX and γ′/γ″ precipitates in the nickel-based superalloy 718 produced by electron beam melting. Mater Sci Eng, A 480(1–2):138–147
Chang SH, Lee SC, Tang TP, Ho HH (2006) Evaluation of HIP pressure on Inconel 718 superalloy. Int J Cast Met Res 19(3):181–187
Acknowledgements
Dr. Eric Tam and Dr. Yiming Yao, Chalmers University of Technology, are acknowledged for their help with XRD and SEM measurements, respectively. Financial assistance by the KK Foundation (20160281) is gratefully acknowledged.
Author information
Authors and Affiliations
Corresponding author
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2018 The Minerals, Metals & Materials Society
About this paper
Cite this paper
Goel, S., Olsson, J., Ahlfors, M., Klement, U., Joshi, S. (2018). The Effect of Location and Post-treatment on the Microstructure of EBM-Built Alloy 718. In: Ott, E., et al. Proceedings of the 9th International Symposium on Superalloy 718 & Derivatives: Energy, Aerospace, and Industrial Applications. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-319-89480-5_6
Download citation
DOI: https://doi.org/10.1007/978-3-319-89480-5_6
Published:
Publisher Name: Springer, Cham
Print ISBN: 978-3-319-89479-9
Online ISBN: 978-3-319-89480-5
eBook Packages: Chemistry and Materials ScienceChemistry and Material Science (R0)