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2014, vol. 64, br. 6, str. 473-486
Određivanje sadržaja pseudoefedrina, paracetamola i askorbinske kiseline u peroralnom prašku primenom reverzno-fazne tečne hromatografije
Univerzitet u Beogradu, Farmaceutski fakultet, Institut za farmaceutsku hemiju i analitiku lekova, Srbija

e-adresaandja@pharmacy.bg.ac.rs
Projekat:
Modelovanje različitih hromatografskih sistema sa hemometrijskim pristupom u farmaceutskoj analizi (MPNTR - 172052)

Ključne reči: pseudoefedrin; paracetamol; askorbinska kiselina RP-HPLC metoda; validacija
Sažetak
Za istovremenu analizu trokomponentne smeše koja sadrži pseudoefedrin, paracetamol i askorbinsku kiselinu postavljene su dve metode reverzno-fazne tečne hromatografije pod visokim pritiskom (RP-HPLC). Hromatografski sistem Hewlett Packard 1100 koji čini HP 1100 binarna pumpa, HP 1100 UV-VIS detektor i HP ChemStation za automatsku obradu podataka korišćen je za hromatografsko razdvajanje. Postupak je obuhvatio definisanje hromatografskih uslova, validaciju postavljenih metoda, kao i njihovu primenu za ispitivanje sadržaja pseudoefedrina, paracetamola i askorbinske kiseline u peroralnom prašku. Optimalna separacija postignuta je u koloni Platinium Alltech Amino 150 mm x 4,6 mm, 5 mm veličine čestica, na temperaturi kolone od 30°C. Volumen injektovanja bio je 20 mL. Mobilna faza u metodi I bila je smeša metanol-voda (30:70 V/V), pH vrednost podešena na 2,5, a u metodi II smeša metanol-voda (60:40 V/V), pH vrednost podešena na 2,9. pH mobilne faze je podešavan sa 85%-tnom orto-fosfornom kiselinom. Talasna dužina detekcije bila je 214 nm u metodi I i 257 nm u metodi II. Protok mobilne faze za obe metode bio je 1 mL min-1. Postavljene metode su validirane i na osnovu dobijenih parametara procenjeno je da obe predložene metode mogu da se primene za analizu peroralnog praška koji sadrži paracetamol, pseudoefedrin i askorbinsku kiselinu.
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O članku

jezik rada: srpski
vrsta rada: stručni članak
DOI: 10.5937/arhfarm1406473M
objavljen u SCIndeksu: 26.05.2015.

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