Published February 20, 2018 | Version v1
Dataset Open

Raw diffraction images of cross-linked cypovirus polyhedra mutant crystals

  • 1. School of Life Science and Technology, Tokyo Institute of Technology
  • 2. RIKEN SPring-8 Center

Description

Diffraction images of cross-linked cypovirus polyhedra mutant crystals related to PDB codes 5YR1, 5YR9, 5YRA, 5YRB, 5YRC, and 5YRD (Negishi et al. 2018, Chem. Commun.).

Small-wedge (5° or 10°/crystal) datasets were collected from loop-harvested microcrystals at a wavelength of 1 Å on BL32XU and BL41XU, SPring-8. The datasets for 5YR1, 5YR9, 5YRB, and 5YRC were collected automatically using ZOO system.

The crystals belonged to space group I23 with unit cell parameter a~103 Å. All datasets were processed and merged using KAMO pipeline with XDS.

This entry includes following data:

  • 1-PhC (5YR1, 1.72 Å)

    • BL32XU (EIGER X 9M)

    • 5°/crystal ×32 (0.1°/frame)

  • 2-PhC (5YR9, 1.70 Å)

    • BL32XU (MX-225HS)

    • 5°/crystal × 127 (1°/frame)

  • 3-PhC (5YRA, 1.79 Å)

    • BL41XU (PILATUS3 6M)

    • 5° or 10°/crystal × 49 (0.25°/frame)

  • ox1-PhC (5YRB, 1.65 Å)

    • BL32XU (EIGER X 9M)

    • 5°/crystal × 78 (0.1°/frame)

  • ox2-PhC (5YRC, 1.67 Å)

    • BL32XU (MX-225HS)

    • 5°/crystal × 323 (1°/frame)

  • ox3-PhC (5YRD, 1.85 Å)

    • BL41XU (PILATUS3 6M)

    • 5°/crystal × 29 (0.25°/frame)

NOTE that EIGER's master.h5 files were modified; see https://github.com/keitaroyam/yamtbx/blob/master/doc/eiger-en.md.

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