Open Access, Peer-reviewed, Quarterly
pISSN 0301-2875
eISSN 2005-3789
    J Korean Acad Prosthodont. 2015 Oct;53(4):318-324. Korean.
    Published online Oct 28, 2015.
    https://doi.org/10.4047/jkap.2015.53.4.318
    Copyright © 2015 The Korean Academy of Prosthodontics
    Original Article

    Evaluation of shear-bond strength between different self-adhesive resin cements with phosphate monomer and zirconia ceramic before and after thermocycling

    Ji-Hun Lee, Min-Kyung Kim, Jung-Jin Lee, Seung-Geun Ahn, Ju-Mi Park and Jae-Min Seo
      • Department of Prosthodontics, School of Dentistry and Institute of Oral Bio-Science, Chonbuk National University, Jeonju, Republic of Korea.
    • Corresponding Author: Jae-Min Seo. Department of Prosthodontics, School of Dentistry and Institute of Oral Bio-Science, Chonbuk National University, 20, Geonji-ro, Deokjin-gu, Jeonju, Jeonbuk 54907, Repulic of Korea. +82 63 250 2696: Email: jmseo@jbnu.ac.kr
    Received July 17, 2015; Revised August 19, 2015; Accepted August 19, 2015.

    This is an Open Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/by-nc/3.0/) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.

    Abstract

    Purpose

    This study compared shear bond strengths of five self-adhesive cements with phosphate monomer to zirconium oxide ceramic with and without airborn particle abrasion.

    Materials and methods

    One hundred zirconia samples were air-abraded (50 µm Al2O3). One hundred composite resin cylinders were fabricated. Composite cylinders were bonded to the zirconia samples with either Permacem 2.0 (P), Clearfil™ SA Luting (C), Multilink® Speed (M), RelyX™ U200 Automix (R), G-Cem LinkAce™ (G). All bonded specimens were stored in distilled water (37℃) for 24 h and half of them were additionally aged by thermocycling (5℃, 55℃, 5,000 times). The bonded specimens were loaded in shear force until fracture (1 mm/min) by using Universal Testing Machine (Model 4201, Instron Co, Canton, MA, USA). The failure sites were inspected under field-emission scanning electron microscopy. The data was analyzed with ANOVA, Tukey HSD post-hoc test and paired samples t-test (α=.05).

    Results

    Before and after thermocycling, Multilink® Speed (M) revealed higher shear-bond strength than the other cements. G-Cem LinkAce™ (G) showed significantly lower bond strengths after thermocycling than before treatment (P<.05), but the other groups were not significantly different (P>.05).

    Conclusion

    Most self-adhesive cements with phosphate monomer showed high shear bond strength with zirconia ceramic and weren't influenced by thermocycling, so they seem to valuable to zirconia ceramic bonding.

    Keywords
    Self-adhesive resin cements; Phosphate monomer; Zirconia ceramic; Shear bond strength; Thermocycling

    Figures

    Fig. 1
    Zirconia specimen.

    Fig. 2
    Composite resin cylinder.

    Fig. 3
    Mean shear bond strength (*: Statistically significant with P<.05).

    Fig. 4
    Failure mode before and after thermocycling (-1 : before thermocycling, -2 : after thermocycling).

    Fig. 5
    Scanning electron microscope image of zirconia surface (×5,000 magnification). (A) polished with 1 µm diamond paste, (B) sandblasting with 50 µm Al2O3.

    Fig. 6
    Scanning electron microscope image of zirconia surface after shear-bond strength test (×2,000 magnification, -1: before thermocycling, -2: after thermocycling). (A) P: Permacem 2.0, (B) C: Clearfil™SA Luting, (C) M: Multilink® Speed, (D) R: RelyX™U200, (E) G: G-Cem LinkAce™

    Tables

    Table 1
    Self-adhesive resin cements used in this study

    Table 2
    Mean shear bond strength (MPa) with SD

    Table 3
    The results of Tukey HSD post hoc test (before thermocycling)

    Table 4
    The results of Tukey HSD post hoc test (after thermocycling)

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    MeSH Terms
    Ceramics*
    Microscopy, Electron, Scanning
    Resin Cements*
    Water
    Zirconium
    Metrics
    Share
    Figures
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    Tables
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