Synthesis and Characterization of Cullet-Clay-Titanium Nitride Ceramic

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Abstract:

A series of ceramic based on (x) titanium nitride- (60-x) cullet-40 kaolin clay, (where 0≤x≤6 wt%) has successfully been made by dry pressing technique followed by sintering at 1000 o C. The actual composition of ceramic is analyzed using Energy Dispersive of X-Ray (EDAX) while the phase existence is determined using X-Ray Diffraction (XRD) technique. Their microstructural morphology is observed under Field Emission Scanning Electron Microscope (FESEM) and the physical properties are determine in term of their density and hardness. It is found that the ceramic contain mostly of Silica and the phase occurrence is dominated by two major phases namely, quartz and tridymite. The structural morphology is observed to be in the form of dendrite structure, with the size become larger as cullet content is decreased. The density is found in the range of 1.941-3.019gcm -3 while the hardness is in the range of 1.174-1.773GPa depending on composition level.

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Periodical:

Solid State Phenomena (Volume 268)

Pages:

128-131

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Online since:

October 2017

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