Synthesis of 7-hydroxy-4-methyl Coumarin with Microwave Radiation Catalyzed by Zirconium Sulfate Tetrahydrate

Shu Jing Liu; Yun Peng Li; Xiu Min Yang; Qing Mei Jiang

doi:10.4028/www.scientific.net/AMR.671-674.2692

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 671-674Synthesis of 7-hydroxy-4-methyl Coumarin with...

Synthesis of 7-hydroxy-4-methyl Coumarin with Microwave Radiation Catalyzed by Zirconium Sulfate Tetrahydrate

Abstract:

The 1,3-benzenediol and ethyl acetoacetate as raw materials were used to synthesize 7-hydroxy-4-methyl coumarin under microwave irradiation with Zirconium sulfate tetrahydrate as the catalyst. The effect of various reaction conditionson on the yield was explored.Experiment shows that the yield reached up to 87. 5%,when the reaction conditions are as follow:n(1,3-benzenediol):n(ethyl acetoacetate)1.0, Zirconium sulfate tetrahydrate 0.4g,10mL cyclohexane, the reaction time 12 min,microwave radiation power 500W.