Dental Materials Journal
Online ISSN : 1881-1361
Print ISSN : 0287-4547
ISSN-L : 0287-4547
Original Paper
A novel coating layer on zirconia using modified zinc phosphatizing method
Kouta KODAMAAlireza VALANEZHADMohammad KHODAEISirus SAFAEEShiva JAFARNIAMahdis NESABIShigeaki ABEIkuya WATANABEHiroshi MURATA
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2021 Volume 40 Issue 4 Pages 870-876

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Abstract

Yttria doped ZrO2 was deposited using an acidic zinc phosphatizing solution and the hydrothermal treatment. The coating was analyzed using a field emission-scanning electron microscope (FE-SEM), X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDX) and X-ray photoelectron spectroscopy (XPS). A piston on three balls (ISO 6872) was used for the measurement of biaxial flexural strength. MC3T3-E1 cells attachment was evaluated by SEM, and cell proliferation were assessed using MTS assay™. SEM images confirmed that the zinc phosphate coating layer was successfully prepared and fully covered the surface. The measured adhesive strength of the coating was 79.11 MPa. In vitro cell study indicated that the coated sample had better cell morphology and proliferation. XRD and EDS analysis revealed that the crystalline coating structure indexed as zinc phosphate (hopeite) and the substrate was assigned as zirconia. The flexural strength test showed that the strength of zirconia before and after hydrothermal treatment was not affected.

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© 2021 The Japanese Society for Dental Materials and Devices
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