Holographic Recording of Unslanted Volume Transmission Gratings in Acrylamide/Propargyl Acrylate Hydrogel Layers: Towards Nucleic Acids Biosensing
Abstract
:1. Introduction
2. Results and Discussions
Biofunctionalization of VTGs and Hybridization Assays by Fluorescence Detection
3. Conclusions
4. Materials and Methods
4.1. Materials
4.2. Hydrogel Layers Preparation
4.3. Morphology Characterization
4.4. Swelling Behavior Studies
4.5. Incubation Step before Recording
4.6. Holographic Recording and Probe Set-Up
4.7. Holographic Recording and Characterization of Hydrogel Layers
4.8. Biofuncionalization of VTGs and Hybridization/Dehybridization Experiments
Supplementary Materials
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Incubation Time (Days) | Layer Thickness (µm) | Recording Beams Intensity (mW/cm2) | Recording Exposure Time (s) | Maximum DE Achieved (%) |
---|---|---|---|---|
1 | 300 | 7.5 | 100 | 40 |
2 | 300 | 7.5 | 100 | 80 |
3 | 300 | 7.5 | 100 | 50 |
VTG Thickness (µm) | Refractive Index Modulation (RIM) | |
---|---|---|
After recording | 190 | 0.0010 |
First washing | 60 | 0.0015 |
Second washing | 62 | 0.0017 |
Incubation Solution | AM (g) | MBA (g) | TEA (mL) | EB (mL) |
---|---|---|---|---|
A | 1 | 0.2 | 1 | 4 |
B | 2 | 0.4 | 1 | 4 |
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Zezza, P.; Lucío, M.I.; Naydenova, I.; Bañuls, M.-J.; Maquieira, Á. Holographic Recording of Unslanted Volume Transmission Gratings in Acrylamide/Propargyl Acrylate Hydrogel Layers: Towards Nucleic Acids Biosensing. Gels 2023, 9, 710. https://doi.org/10.3390/gels9090710
Zezza P, Lucío MI, Naydenova I, Bañuls M-J, Maquieira Á. Holographic Recording of Unslanted Volume Transmission Gratings in Acrylamide/Propargyl Acrylate Hydrogel Layers: Towards Nucleic Acids Biosensing. Gels. 2023; 9(9):710. https://doi.org/10.3390/gels9090710
Chicago/Turabian StyleZezza, Paola, María Isabel Lucío, Izabela Naydenova, María-José Bañuls, and Ángel Maquieira. 2023. "Holographic Recording of Unslanted Volume Transmission Gratings in Acrylamide/Propargyl Acrylate Hydrogel Layers: Towards Nucleic Acids Biosensing" Gels 9, no. 9: 710. https://doi.org/10.3390/gels9090710