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Studies on the base catalyzed synthesis of acetophenone enolcarbamate enhanced by microwaves
Published:
30 November 2006
by MDPI
in The 10th International Electronic Conference on Synthetic Organic Chemistry
session Symposium on Microwave Assisted Synthesis
Abstract: Microwave assisted organic synthesis (MAOS) of N,N-diisopropyl enol carbamate of acetophenone is achieved in good yield when acetophenone, N,N-diisopropylcarbamoyl chloride and Hüning's base, DABCO or TMEDA were irradiated with microwaves. It is remarkable that reaction times are reduced from six days with conventional heating, to twenty minutes.
Keywords: n/a
