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Licensed Unlicensed Requires Authentication Published by De Gruyter July 9, 2015

Microstructural characterization of nanostructured supersonic sprayed Ni–Sn coatings after wear tests at elevated temperature

Paper presented at “XV International Conference on Electron Microscopy”, 15–18 September 2014, Cracow, Poland

  • Jan Kusinski , Slawomir Kac , Kazimierz Kowalski , Beata Dubiel , Stanislaw Dymek , Aleksandra Czyrska-Filemonowicz , Sergi Dosta , Jean-Pierre Celis , Emmanuel Georgiou and Paolo Matteazzi

Abstract

The paper presents results of the wear behavior, as well as the microstructural (scanning and transmission electron microscopy) and compositional (microanalysis with using energy dispersive and X-ray photon emission spectroscopy) characterization of nanostructured Ni-20Sn (wt.%) coatings, deposited on an Inconel 718 substrate by supersonic cold gas spraying at different spraying parameters. Coatings were examined in the as-deposited state and after testing in a linearly reciprocating sliding wear test at room temperature, 200, 400 and 550 °C. It was found that the Ni–Sn coatings exhibit superior wear resistance compared to benchmark materials. This is attributed to an appropriate balance of soft (Ni) and to hard (Ni3Sn – intermetallic) phases and to the nanostructure of the matrix, as well as to the presence of an NiO oxide tribo-layer, as revealed by the microanalysis and electron microscopy.


*Correspondence address, Prof. Jan Kusinski, AGH University of Science and Technology, 30 Mickiewicza Ave., 30-059 Krakow, Poland, Tel.: +48-12-617 3344, Fax: +48-12-617 2639, E-mail:

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Received: 2014-10-29
Accepted: 2015-01-27
Published Online: 2015-07-09
Published in Print: 2015-07-04

© 2015, Carl Hanser Verlag, München

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