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Licensed Unlicensed Requires Authentication Published by De Gruyter 2021

Thermomechanical properties of forcespun polycaprolactone fibers infused with fish scale-based hydroxyapatite

From the book Plant and Animal Based Composites

  • Deepa Kodali , Vincent Hembrick-Holloman , Shaik Jeelani and Vijaya K. Rangari

Abstract

Biomaterials synthesized from natural resources have attracted plentitude of attention over the past few decades. Hydroxyapatite (HA) is one such biomaterial with excellent characteristics suitable for biomedical applications. In this study, HA is synthesized from carpa fish scales by calcination method. The HA particles were nanomilled for particle size reduction and these particles were characterized using X-ray diffraction, scanning electron microscopy and transmission electron microscopy. A novel forcespinning technique was used to fabricate microfibers from polycaprolactone (PCL) infused with synthesized HA. Thermomechanical properties of the PCL/HA fiber mats were investigated using differential scanning calorimetry, dynamic mechanical analysis and tensile tests. The analyses suggest that infusing HA in moderate quantities enhances the thermomechanical properties of composite fibers.

© 2021 Walter de Gruyter GmbH, Berlin/Munich/Boston
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