Synthesis and Crystal Structure of the Copper Complex Based on Aza-crown Ether containing Nicotinic acidChinese Full Text
GONG Wei-jie;ZHOU Yang;College of science and technology,Qiongzhou University;
Abstract: A novel 1D chain supramolecular copper coordination polymer has been designed and synthesized based on the coordination ability of nicotinic acid. The crystal structure of the compound was determined by X-ray diffraction method. The results revealed that it belongs to triclinic system,space group P-1 with a = 8. 400（ 5） ,b = 14.093（ 5） ,c =18.257（ 5）; α =93.517（ 5） °,β = 97.787（ 5） °,γ = 98.029（ 5） °; Z =2,V= 2113. 3（ 16） 3,Dc= 1. 484 mg /m3,F（ 000） =984,R1 =0.0546,wR2 =0.1711. The complex shows a 1D chain in the packing structure through hydrogen bonding.
- DOI：
10.13307/j.issn.1008-6722.2014.05.10
- Series：
- Subject：
- Classification Code：
O627.12
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