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A Novel Strategy to Fabricate CuS, Cu7.2S4, and Cu2 – xSe Nanofibers via Inheriting the Morphology of Electrospun CuO Nanofibers

  • PHYSICAL CHEMISTRY OF NANOCLUSTERS AND NANOMATERIALS
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Abstract

CuO nanofibers were fabricated by calcination of the electrospun PVP/Cu(NO3)2 composite nanofibers. For the first time, CuS, Cu7.2S4, and Cu2 – xSe nanofibers were successfully synthesized by double-crucible sulfurization and selenidation methods via inheriting the morphology of CuO nanofibers as precursors, respectively. X-ray diffraction (XRD) analysis shows CuS, Cu7.2S4, and Cu2 – xSe nanofibers are respectively pure hexagonal phase, cubic phase and orthorhombic phase with space group of P63/mmc, Fm-3m and Cmcm. Scanning electron microscopy (SEM) indicates that the diameter of CuS, Cu7.2S4, and Cu2 – xSe nanofibers are 149.60 ± 17.52, 103.40 ± 12.95, and 127.28 ± 19.55 nm under the 95% confidence level, respectively. More importantly, this preparation technique is of universal significance to prepare other metal chalcogenides nanofibers.

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ACKNOWLEDGMENTS

This work was financially supported by National Natural Science Foundation of China (51573023, 50972020), Natural Science Foundation of Jilin Province (20170101101JC), Industrial Technology Research and Development Project of Jilin Province Development and Reform Commission (2017C051), Science and Technology Research Planning Project of the Education Department of Jilin Province during the 13th Five-Year Plan Period (JJKH20170608KJ), Youth Foundation of Changchun University of Science and Technology (no. XQNJJ-2016-01).

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Authors and Affiliations

  1. Key Laboratory of Applied Chemistry and Nanotechnology at Universities of Jilin Province, Changchun University of Science and Technology, 130022, Changchun, China

    Li Cheng, Dan Li, Wensheng Yu, Qianli Ma, Xiangting Dong, Xinlu Wang, Jinxian Wang & Guixia Liu

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  1. Li Cheng
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  2. Dan Li
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  3. Wensheng Yu
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  6. Xinlu Wang
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Correspondence to Wensheng Yu or Xiangting Dong.

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Li Cheng, Li, D., Yu, W. et al. A Novel Strategy to Fabricate CuS, Cu7.2S4, and Cu2 – xSe Nanofibers via Inheriting the Morphology of Electrospun CuO Nanofibers. Russ. J. Phys. Chem. 93, 730–735 (2019). https://doi.org/10.1134/S0036024419040198

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