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Synthesis of Mg(Fe0.8Ga0.2)2O4 by Gel Combustion Using Glycine and Starch

  • Synthesis and Properties of Inorganic Compounds
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Abstract

A powdery material Mg(Fe0.8Ga0.2)2O4 has been prepared by combusting a gel containing magnesium(II), iron(III), and gallium(III) nitrates and a glycine–starch mixture. The gel produced during the synthesis has been studied by thermal analysis (TGA/DSC) and IR spectroscopy. This mixture has been shown to be efficient to produce a homogeneous nanosized powderlike material Mg(Fe0.8Ga0.2)2O4. The morphology and properties of ceramic samples are characterized by scanning electron microscopy, X-ray powder diffraction, neutron diffraction, and vibrational magnetometry.

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Moscow, 119991, Russia

    M. N. Smirnova, M. A. Kop’eva, E. N. Beresnev, L. V. Goeva, N. P. Simonenko, G. E. Nikiforova & V. A. Ketsko

  2. Scientific and Practical Materials Research Center, National Academy of Sciences of Belarus, Minsk, 220072, Belarus

    A. V. Trukhanov

Authors
  1. M. N. Smirnova
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  2. M. A. Kop’eva
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  3. E. N. Beresnev
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  4. L. V. Goeva
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  5. N. P. Simonenko
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  6. G. E. Nikiforova
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  7. A. V. Trukhanov
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  8. V. A. Ketsko
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Corresponding author

Correspondence to M. N. Smirnova.

Additional information

Original Russian Text © M.N. Smirnova, M.A. Kop’eva, E.N. Beresnev, L.V. Goeva, N.P. Simonenko, G.E. Nikiforova, A.V. Trukhanov, V.A. Ketsko, 2018, published in Zhurnal Neorganicheskoi Khimii, 2018, Vol. 63, No. 10, pp. 1239–1243.

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Smirnova, M.N., Kop’eva, M.A., Beresnev, E.N. et al. Synthesis of Mg(Fe0.8Ga0.2)2O4 by Gel Combustion Using Glycine and Starch. Russ. J. Inorg. Chem. 63, 1257–1261 (2018). https://doi.org/10.1134/S0036023618100182

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  • DOI: https://doi.org/10.1134/S0036023618100182

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