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Characterization and Crystal Structure of a Novel Mononuclear Cobalt(II) Complex with Hydrazone Derived from Protocatechuic Acid

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Abstract

A novel complex [CoII(L)2·CH3OH] with hydrazone derived from protocatechuic acid (HL=C16H14N2O4) is designed and synthesized. The complex is characterized by single crystal X-ray diffraction, elemental analysis, IR, and thermal gravimetric analysis. The complex crystallizes in the monoclinic space group C2/c, with unit cell dimensions a = 25.1715(11), b = 9.3518(4), c = 12.8700(6) Å, β = 103.6530(10)°, V = 2943.98(75) Å3, Z = 4, R1 = 0.0612, and wR2 = 0.1439.

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Authors and Affiliations

  1. School of Life Sciences, Shandong University of Technology, Shandong, P. R. China

    G.-H. Sheng, C.-F. Wang, S. Feng, X. Gao & H.-L. Zhu

Authors
  1. G.-H. Sheng
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  2. C.-F. Wang
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  3. S. Feng
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  4. X. Gao
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  5. H.-L. Zhu
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Corresponding author

Correspondence to H.-L. Zhu.

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Original Russian Text © 2018 G.-H. Sheng, C.-F. Wang, S. Feng, X. Gao, H.-L. Zhu.

The text was submitted by the authors in English. Zhurnal Strukturnoi Khimii, Vol. 59, No. 1, pp. 144–148, January–February, 2018.

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Sheng, GH., Wang, CF., Feng, S. et al. Characterization and Crystal Structure of a Novel Mononuclear Cobalt(II) Complex with Hydrazone Derived from Protocatechuic Acid. J Struct Chem 59, 140–144 (2018). https://doi.org/10.1134/S0022476618010213

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  • DOI: https://doi.org/10.1134/S0022476618010213

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