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Crystal structure of N′-pivaloyl-N-phenylpivalohydrazide

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Abstract

A novel hydrazide compound (C16H24N2O2) is synthesized in a single step by the reaction of pivaloyl chloride with phenylhydrazine in a 2:1 molar ratio in dry DCM. The molecular structure is determined by the single crystal X-ray analysis. The compound crystallized in the monoclinic system, space group P21/c with a = 15.4638(17) Å, b = 9.9481(11) Å, c = 10.5276(12) Å, β = 90.194(3)°, Z = 4, V = 1619.5(3) Å3.

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Authors and Affiliations

  1. Department of Chemistry, Quaid-I-Azam University, Islamabad, Pakistan

    A. Saeed & I. Arshad

  2. Department of Inorganic and Analytical Chemistry, Universität Paderborn, Paderborn, Germany

    U. Flörke

Authors
  1. A. Saeed
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  2. I. Arshad
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  3. U. Flörke
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Correspondence to U. Flörke.

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Original Russian Text © 2015 A. Saeed, I. Arshad, U. Flörke.

The text was submitted by the authors in English. Zhurnal Strukturnoi Khimii, Vol. 56, No. 2, pp. 414–416, March–April, 2015.

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Saeed, A., Arshad, I. & Flörke, U. Crystal structure of N′-pivaloyl-N-phenylpivalohydrazide. J Struct Chem 56, 396–398 (2015). https://doi.org/10.1134/S0022476615020304

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  • DOI: https://doi.org/10.1134/S0022476615020304

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